1,2-Benzenedicarbonitrile, 3,6-bis(1-methylethoxy)-

Base Information

Chemical Name:1,2-Benzenedicarbonitrile, 3,6-bis(1-methylethoxy)-
CAS No.:201140-18-3
Molecular Formula:C14H16N2O2
Molecular Weight:244.293
Hs Code.:
DSSTox Substance ID:DTXSID80443158
Wikidata:Q82260869

Synonyms:1,2-Benzenedicarbonitrile, 3,6-bis(1-methylethoxy)-;201140-18-3;DTXSID80443158

Suppliers and Price of 1,2-Benzenedicarbonitrile, 3,6-bis(1-methylethoxy)-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1,2-Benzenedicarbonitrile, 3,6-bis(1-methylethoxy)-

Chemical Property:

XLogP3:2.9
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:4
Exact Mass:244.121177757
Heavy Atom Count:18
Complexity:325

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC(C)OC1=C(C(=C(C=C1)OC(C)C)C#N)C#N

Technology Process of 1,2-Benzenedicarbonitrile, 3,6-bis(1-methylethoxy)-

There total 2 articles about 1,2-Benzenedicarbonitrile, 3,6-bis(1-methylethoxy)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 4733-50-0
2,3-dicyano-1,4-hydroquinone

: 75-26-3
isopropyl bromide

: 201140-18-3
3,6-bis(1-methylethoxy)-1,2-benzenedicarbonitrile

Guidance literature:: With potassium carbonate; In N,N-dimethyl-formamide; at 60 ℃; for 48h;
DOI:10.1021/jo971683c

Reference yield:

: 642-96-6
1,2,3,4-tetrahydroxybenzene

: 75-26-3
isopropyl bromide

: 201140-18-3
3,6-bis(1-methylethoxy)-1,2-benzenedicarbonitrile

Guidance literature:: With potassium carbonate; In N,N-dimethyl-formamide; at 60 ℃; Inert atmosphere;
DOI:10.1016/j.dyepig.2014.05.013

Reference yield:

: 201140-18-3
3,6-bis(1-methylethoxy)-1,2-benzenedicarbonitrile

: C₆₈H₆₀N₈O₂S₆

Guidance literature:: Multi-step reaction with 2 steps

1: 85 percent / Na, NH₃ / ethane-1,2-diol / 5 h / 140 - 150 °C

2: 1.) Mg(OBu)2, 2.) AcOH / 1.) BuOH, refllux, 6 h, 2.) CH₂Cl₂, 0 deg C, 30 min

With ammonia; sodium; magnesium di-n-butanolate; acetic acid; In ethylene glycol;
DOI:10.1021/jo971683c