N,N'-bis(acetylacetone)-1,2-ethylenediimine

Base Information

Chemical Name:N,N'-bis(acetylacetone)-1,2-ethylenediimine
CAS No.:52751-14-1
Molecular Formula:C₁₂H₂₀N₂O₂
Molecular Weight:224.303
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N,N'-bis(acetylacetone)-1,2-ethylenediimine

Chemical Property:

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Technology Process of N,N'-bis(acetylacetone)-1,2-ethylenediimine

There total 1 articles about N,N'-bis(acetylacetone)-1,2-ethylenediimine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 89376-43-2
4-[(2-aminoethyl)amino]pent-3-en-2-one

: 2161-87-7
1,3,5-triacetyl-2,4,6-trihydroxybenzene

: 2,4,6-tris{1-[2-(1-methyl-1-en-3-one-butylamino)ethylimino]ethyl}-1,3,5-trihydroxybenzene

: 52751-14-1
N,N'-bis(acetylacetone)-1,2-ethylenediimine

Guidance literature:: for 18h;
DOI:10.1016/j.ica.2010.06.054

Reference yield:

: 52751-14-1
N,N'-bis(acetylacetone)-1,2-ethylenediimine

: dibenzyltin oxide

: Sn(CH₂C₆H₅)2(CH₃COHCHC(CH₃)NCH₂CH₂NC(CH₃)CHCOCH₃)2*2H₂O

Guidance literature:: With H₂O; In ethanol; benzene; ligand and Sn-compound (2:1) were refluxed in a mixt. of C6H6 and EtOH for 2 h; filtered, evapd., dried under vac. for 1 h; elem. anal.;

Reference yield:

: 92622-25-8
n-butylammonium tetrachlorooxotechnetate(V)

: 52751-14-1
bis(acetylacetone)ethylenediimine

: 3109-63-5
tert-butylammonium hexafluorophosphate(V)

: 1605-53-4
diethyl-phenyl-phosphine

: 93427-00-0
trans-bis(phenyldiethylphosphine)(N,N'-ethylenebis(acetylacetone iminato))technetium(III) hexafluorophosphate

Guidance literature:: In methanol; Schiff base ligand adding to soln. of Tc complex; stirring for ca 15 min, phosphine adding, stirring for 15 min at room temp., filtration, evapn., dissoln. in CH2Cl2, chromy. on silica (CH2Cl2, then Me2CO, then MeOH), addn. of Bu4NPF6 to last fraction; cooling, collection of product, washing with H2O, drying in vac. over P2O5;