11-Methyltridecan-1-OL

Base Information

• Chemical Name: 11-Methyltridecan-1-OL
• CAS No.: 20194-46-1
• Molecular Formula: C14H30O
• Molecular Weight: 214.392
• DSSTox Substance ID: DTXSID70592846
• Nikkaji Number: J1.763.976E
• Mol file: 20194-46-1.mol

Synonyms:11-METHYLTRIDECAN-1-OL;20194-46-1;SCHEMBL5702185;DTXSID70592846

Chemical Property of 11-Methyltridecan-1-OL

Chemical Property:

• XLogP3: 5.9
• Hydrogen Bond Donor Count: 1
• Hydrogen Bond Acceptor Count: 1
• Rotatable Bond Count: 11
• Exact Mass: 214.229665576
• Heavy Atom Count: 15
• Complexity: 112

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CCC(C)CCCCCCCCCCO

Technology Process of 11-Methyltridecan-1-OL

There total 1 articles about 11-Methyltridecan-1-OL which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

9-bromononan-1-ol (55362-80-6) → 11-methyl-1-tridecanol (20194-46-1)

Guidance literature:

Multi-step reaction with 4 steps

1: 100 percent / p-toluenesulfonic acid / CHCl₃

2: 45 percent / Heating

3: 1.) n-BuLi / 1.) THF, DMSO, hexane, RT, 30 min, 2.) THF, DMSO, hexane, RT, 3 h

4: 100 percent / H₂ / PtO₂ / methanol / Ambient temperature

With n-butyllithium; hydrogen; toluene-4-sulfonic acid; platinum(IV) oxide; In methanol; chloroform;

DOI:10.1021/jo00364a024

Reference yield:

11-methyl-1-tridecanol (20194-46-1) + (-)-chloromenthyloxydiphenylsilane (67131-32-2) → ((1R,2S,5R)-2-Isopropyl-5-methyl-cyclohexyloxy)-(11-methyl-tridecyloxy)-diphenyl-silane

Guidance literature:

DOI:10.1021/ol049233b

Reference yield:

11-methyl-1-tridecanol (20194-46-1) + (+)-chloromenthoxydiphenylsilane (290307-79-8) → ((1S,2R,5S)-2-Isopropyl-5-methyl-cyclohexyloxy)-(11-methyl-tridecyloxy)-diphenyl-silane

Guidance literature:

DOI:10.1021/ol049233b

upstream raw materials:

9-bromononan-1-ol