4-Dimethylaminocyclohexanone oxime

Base Information

Chemical Name:4-Dimethylaminocyclohexanone oxime
CAS No.:203985-55-1
Molecular Formula:C8H16N2O
Molecular Weight:156.228
Hs Code.:
DSSTox Substance ID:DTXSID90446716

Synonyms:203985-55-1;4-(Dimethylamino)cyclohexanoneoxime;4-dimethylaminocyclohexanone oxime;4-(Dimethylamino)cyclohexanone oxime;Cyclohexanone, 4-(dimethylamino)-, oxime;SCHEMBL6961918;DTXSID90446716;ORARBYAEFARIRC-UHFFFAOYSA-N

Suppliers and Price of 4-Dimethylaminocyclohexanone oxime

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 1 raw suppliers

Chemical Property of 4-Dimethylaminocyclohexanone oxime

Chemical Property:

XLogP3:0.8
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:1
Exact Mass:156.126263138
Heavy Atom Count:11
Complexity:144

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CN(C)C1CCC(=NO)CC1

Technology Process of 4-Dimethylaminocyclohexanone oxime

There total 4 articles about 4-Dimethylaminocyclohexanone oxime which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 40594-34-1
4-(dimethylamino)cyclohexanone

: 203985-55-1
4-dimethylaminocyclohexanone oxime

Guidance literature:: With pyridine; hydroxylamine hydrochloride; In ethanol; for 3h; Heating;
DOI:10.1021/jo020600b

Reference yield:

: 4-dimethylaminocyclohexanone hydrochloride

: 203985-55-1
4-dimethylaminocyclohexanone oxime

Guidance literature:: With pyridine; hydroxylamine hydrochloride; potassium carbonate; In ethanol; water;

Reference yield:

: 4746-97-8
cyclohexanedione monoethylene ketal

: 203985-55-1
4-dimethylaminocyclohexanone oxime

Guidance literature:: Multi-step reaction with 3 steps

1: glacial acetic acid; sodium triacetoxyborohydride / CH₂Cl₂; tetrahydrofuran / 10 - 20 °C

2: 119 g / hydrochloric acid / H₂O / 1 h / Heating

3: 87 percent / hydroxylamine hydrochloride; pyridine / ethanol / 3 h / Heating

With pyridine; hydrogenchloride; hydroxylamine hydrochloride; sodium tris(acetoxy)borohydride; acetic acid; In tetrahydrofuran; ethanol; dichloromethane; water;
DOI:10.1021/jo020600b