1,10-Phenanthroline, 2-(2,4,6-trimethylphenyl)-

Base Information

• Chemical Name: 1,10-Phenanthroline, 2-(2,4,6-trimethylphenyl)-
• CAS No.: 204195-45-9
• Molecular Formula: C21H18N2
• Molecular Weight: 298.387
• Mol file: 204195-45-9.mol

Synonyms:

Chemical Property of 1,10-Phenanthroline, 2-(2,4,6-trimethylphenyl)-

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 1,10-Phenanthroline, 2-(2,4,6-trimethylphenyl)-

There total 1 articles about 1,10-Phenanthroline, 2-(2,4,6-trimethylphenyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

1,10-Phenanthroline (66-71-7) + 2,4,6-trimethylphenyl bromide (576-83-0) → 2-(2,4,6-trimethylphenyl)[1,10]phenanthroline (204195-45-9)

Guidance literature:

2,4,6-trimethylphenyl bromide; With n-butyllithium;

1,10-Phenanthroline;

With manganese(IV) oxide;

DOI:10.1002/chem.200305770

Reference yield: 85.0%

2-(2,4,6-trimethylphenyl)[1,10]phenanthroline (204195-45-9) + copper(l) iodide (7681-65-4) + sodium hexaflorophosphate → C42H36CuN4(1+)*F6P(1-)

Guidance literature:

2-(2,4,6-trimethylphenyl)[1,10]phenanthroline; copper(l) iodide; In acetonitrile; at 20 ℃; for 0.5h; Inert atmosphere;

sodium hexaflorophosphate; In ethanol; water; for 2h;

DOI:10.1021/acs.inorgchem.7b02323

Reference yield: 72.0%

2-(2,4,6-trimethylphenyl)[1,10]phenanthroline (204195-45-9) + sodium hexaflorophosphate + copper(ll) sulfate pentahydrate → C42H36CuN4(2+)*2F6P(1-)

Guidance literature:

2-(2,4,6-trimethylphenyl)[1,10]phenanthroline; copper(ll) sulfate pentahydrate; In water; at 20 ℃; for 1h;

sodium hexaflorophosphate; In ethanol; water; for 2h;

DOI:10.1021/acs.inorgchem.7b02323

upstream raw materials:

1,10-Phenanthroline

2,4,6-trimethylphenyl bromide

Downstream raw materials:

2,9-dimesityl-[1,10]-phenanthroline

2-(4-methoxy-2,6-dimethylphenyl)-9-(2,4,6-trimethylphenyl)-1,10-phenanthroline

3,5-dimethyl-4-[9-(2,4,6-trimethylphenyl)-1,10-phenanthrolin-2-yl]phenol

(((CH₃)2C₆H₂)2C₁₂H₆N₂CH₃)2O₈(CH₂)12C₆H₄