1-[(p-Bromophenyl)sulfonyl]-1H-azepine

Base Information

• Chemical Name: 1-[(p-Bromophenyl)sulfonyl]-1H-azepine
• CAS No.: 20646-55-3
• Molecular Formula: C₁₂H₁₀BrNO₂S
• Molecular Weight: 312.187
• Hs Code.: 2933990090
• Mol file: 20646-55-3.mol

Synonyms:1-[(4-Bromophenyl)sulfonyl]-1H-azepine;1-[(p-Bromophenyl)sulfonyl]-1H-azepine;N-(4-Bromophenylsulfonyl)-1H-azepine;

Chemical Property of 1-[(p-Bromophenyl)sulfonyl]-1H-azepine

Chemical Property:

• PSA: 45.76000
• LogP: 4.05570

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 1-[(p-Bromophenyl)sulfonyl]-1H-azepine

There total 2 articles about 1-[(p-Bromophenyl)sulfonyl]-1H-azepine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

4-bromobenzenesulfonyl chloride (98-58-8) + benzene (71-43-2,26181-88-4,54682-86-9,13967-78-7,174973-66-1) → N-p-bromobenzenesulphonyl-1H-azepine (20646-55-3)

Guidance literature:

With sodium azide; Aliquat 336; sodium hydrogencarbonate; a) 40 deg C, 3 h, b) 125 deg C, 3 h;

DOI:10.1055/s-1992-26146

Reference yield: 36.2%

p-bromobenzenesulfonyl azide (6647-76-3) + benzene (71-43-2,26181-88-4,54682-86-9,13967-78-7,174973-66-1) → 4-bromo-benzenesulfonic acid amide (701-34-8) + 4-bromo-N-phenylbenzenesulfonamide (7454-54-8) + N-p-bromobenzenesulphonyl-1H-azepine (20646-55-3)

Guidance literature:

at 140 ℃; for 0.666667h; under 41371.8 - 63092.1 Torr; Yield given. Title compound not separated from byproducts;

upstream raw materials:

4-bromobenzenesulfonyl chloride

benzene

p-bromobenzenesulfonyl azide

Post a RFQ

Cas No.:

Product Name:

Quantity:

Please select Metric Ton KG G Pound L ML

Email:

Company name:

Valid Period:

Detailed Requirements:

• Sample
• MOQ
• GMP
• FDA
• Price
  FOB CIF CFR EXW
• Urgent purchase

Enter 15 to 2000 letters.Word count: 0 letters

Attach files(File Format: Jpeg, Jpg, Gif, Png, PDF, PPT, Zip, Rar,Word or Excel Maximum File Size: 3MB)

Remove

Submit

1

What can I do for you?
Get Best Price

Get Best Price for 20646-55-3 1-[(p-Bromophenyl)sulfonyl]-1H-azepine

Send

Send

Metric Ton KG G Pound L ML

Send

Send