2-Azabicyclo[2.2.1]heptane, 2-hydroxy-

Base Information

• Chemical Name: 2-Azabicyclo[2.2.1]heptane, 2-hydroxy-
• CAS No.: 85689-01-6
• Molecular Formula: C6H11 N O
• Molecular Weight: 112.1497
• Hs Code.: 2933990090
• Mol file: 85689-01-6.mol

Synonyms:2-Azabicyclo[2.2.1]heptan-exo-2-ol;2-Azabicyclo(2.2.1)heptane,2-hydroxy;

Chemical Property of 2-Azabicyclo[2.2.1]heptane, 2-hydroxy-

Chemical Property:

• Boiling Point: °Cat760mmHg
• Flash Point: °C
• PSA: 3.24000
• Density: g/cm³
• LogP: 0.75410

Purity/Quality:

99% ^*data from raw suppliers

2-hydroxy-2-Azabicyclo[2.2.1]heptane 97.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2-Azabicyclo[2.2.1]heptane, 2-hydroxy-

There total 2 articles about 2-Azabicyclo[2.2.1]heptane, 2-hydroxy- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-(Benzoyloxy)-2-azabicyclo<2.2.1>heptan (85689-06-1) → 2-aza-bicyclo[2.2.1]heptane (279-24-3) + 2-Azabicyclo<2.2.1>heptan-exo-2-ol (85689-01-6) + 2-Azabicyclo<2.2.1>heptan-endo-2-ol (85689-01-6)

Guidance literature:

With sodium hydroxide; In methanol; at 10 ℃; for 0.5h; Title compound not separated from byproducts;

Reference yield:

2-(Benzoyloxy)-2-azabicyclo<2.2.1>heptan (85689-06-1) → 2-aza-bicyclo[2.2.1]heptane (279-24-3) + 2-Azabicyclo<2.2.1>heptan-exo-2-ol (85689-01-6) + 2-Azabicyclo<2.2.1>heptan-endo-2-ol (85689-01-6)

Guidance literature:

With sodium hydroxide; In methanol; at 10 ℃; for 0.5h; Title compound not separated from byproducts;

Reference yield: 49.0%

methanol (67-56-1) + 2-Azabicyclo<2.2.1>heptan-2-ol (85689-01-6) + p-toluenesulfonyl chloride (98-59-9) → exo-2-Methoxy-1-azabicyclo<2.2.1>heptan (85689-09-4) + exo-2-(4-Methylphenylsulfonyloxy)-1-azabicyclo<2.2.1>heptan (81640-20-2,85689-08-3)

Guidance literature:

With sodium hydroxide; at 0 ℃; for 0.75h; Product distribution; Mechanism; var. of solvent; 18O-, 2H-study;

upstream raw materials:

2-(Benzoyloxy)-2-azabicyclo<2.2.1>heptan

Downstream raw materials:

exo-2-Methoxy-1-azabicyclo<2.2.1>heptan

exo-2-(4-Methylphenylsulfonyloxy)-1-azabicyclo<2.2.1>heptan

exo-2-(4-Methoxyphenylsulfonyloxy)-1-azabicyclo<2.2.1>heptan

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