2--3-methyl-3-carbomethoxy-cyclohexanon

Base Information

• Chemical Name: 2--3-methyl-3-carbomethoxy-cyclohexanon
• CAS No.: 95946-49-9
• Molecular Formula: C₂₀H₂₈O₃
• Molecular Weight: 316.441

Synonyms:

Chemical Property of 2--3-methyl-3-carbomethoxy-cyclohexanon

Chemical Property:

Purity/Quality:

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Technology Process of 2--3-methyl-3-carbomethoxy-cyclohexanon

There total 3 articles about 2--3-methyl-3-carbomethoxy-cyclohexanon which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4-carbethoxy-3-methyl-2-cyclohexen-1-one (487-51-4) → 2--3-methyl-3-carbomethoxy-cyclohexanon (95946-49-9)

Guidance literature:

Multi-step reaction with 2 steps

1: (i) KOtBu, (ii) KOH, EtOH

2: (i), (ii) aq. KOH, (iii) /BRN= 102415/

DOI:10.1016/S0040-4020(01)99353-6

Reference yield:

2-(3-Isopropylphenyl)ethyl Bromide (72646-50-5) → 2--3-methyl-3-carbomethoxy-cyclohexanon (95946-49-9)

Guidance literature:

Multi-step reaction with 2 steps

1: (i) KOtBu, (ii) KOH, EtOH

2: (i), (ii) aq. KOH, (iii) /BRN= 102415/

DOI:10.1016/S0040-4020(01)99353-6

Reference yield:

diazomethane (186581-53-3,908094-01-9,334-88-3) + 2-(3-isopropyl-phenethyl)-3-methyl-cyclohex-2-enone (95157-66-7) + potassium cyanide (151-50-8) → 2--3-methyl-3-carbomethoxy-cyclohexanon (95946-49-9)

Guidance literature:

Multistep reaction; (i), (ii) aq. KOH, (iii) /BRN= 102415/;

DOI:10.1016/S0040-4020(01)99353-6

upstream raw materials:

diazomethane

2-(3-isopropyl-phenethyl)-3-methyl-cyclohex-2-enone

potassium cyanide

4-carbethoxy-3-methyl-2-cyclohexen-1-one

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