1-Chloro-4-methoxy-5-methyl-2-nitrobenzene

Base Information

Chemical Name:1-Chloro-4-methoxy-5-methyl-2-nitrobenzene
CAS No.:20871-70-9
Molecular Formula:C8H8ClNO3
Molecular Weight:201.609
Hs Code.:
DSSTox Substance ID:DTXSID901265222

Synonyms:1-Chloro-4-methoxy-5-methyl-2-nitrobenzene;20871-70-9;SCHEMBL2840001;ABTIOYFAEPUQAA-UHFFFAOYSA-N;DTXSID901265222

Suppliers and Price of 1-Chloro-4-methoxy-5-methyl-2-nitrobenzene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 1 raw suppliers

Chemical Property of 1-Chloro-4-methoxy-5-methyl-2-nitrobenzene

Chemical Property:

XLogP3:2.7
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:1
Exact Mass:201.0192708
Heavy Atom Count:13
Complexity:194

Purity/Quality:: 95% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CC1=CC(=C(C=C1OC)[N+](=O)[O-])Cl

Technology Process of 1-Chloro-4-methoxy-5-methyl-2-nitrobenzene

There total 3 articles about 1-Chloro-4-methoxy-5-methyl-2-nitrobenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 923274-91-3
Ethenesulfonic acid 4-chloro-2-methyl-5-nitrophenyl ester

: 20871-70-9
1-Chloro-4-methoxy-5-methyl-2-nitrobenzene

Guidance literature:: Multi-step reaction with 2 steps

1: ethanol; water; potassium carbonate / 1 h / Heating / reflux

2: potassium carbonate / N,N-dimethyl-formamide / 2 h / 20 °C

With ethanol; water; potassium carbonate; In N,N-dimethyl-formamide;

Reference yield:

: 1570-64-5
2-methyl-4-chlorophenol

: 20871-70-9
1-Chloro-4-methoxy-5-methyl-2-nitrobenzene

Guidance literature:: Multi-step reaction with 4 steps

1: sodium hydroxide / 1,1-dichloroethane; water; acetone / 3 h / Heating / reflux

2: sulfuric acid; nitric acid / 1 h / 5 - 10 °C

3: ethanol; water; potassium carbonate / 1 h / Heating / reflux

4: potassium carbonate / N,N-dimethyl-formamide / 2 h / 20 °C

With sodium hydroxide; ethanol; sulfuric acid; water; nitric acid; potassium carbonate; In 1,1-dichloroethane; water; N,N-dimethyl-formamide; acetone;

Reference yield:

: 4790-38-9
Ethenesulfonic acid 4-chloro-2-methylphenyl ester

: 20871-70-9
1-Chloro-4-methoxy-5-methyl-2-nitrobenzene

Guidance literature:: Multi-step reaction with 3 steps

1: sulfuric acid; nitric acid / 1 h / 5 - 10 °C

2: ethanol; water; potassium carbonate / 1 h / Heating / reflux

3: potassium carbonate / N,N-dimethyl-formamide / 2 h / 20 °C

With ethanol; sulfuric acid; water; nitric acid; potassium carbonate; In N,N-dimethyl-formamide;