Benzene, 1-[(1-chloro-2,2-diphenylethenyl)sulfinyl]-4-methyl-

Base Information

Chemical Name:Benzene, 1-[(1-chloro-2,2-diphenylethenyl)sulfinyl]-4-methyl-
CAS No.:209391-60-6
Molecular Formula:C21H17ClOS
Molecular Weight:352.884
Hs Code.:
DSSTox Substance ID:DTXSID90466717
Nikkaji Number:J1.084.520C

Synonyms:Benzene, 1-[(1-chloro-2,2-diphenylethenyl)sulfinyl]-4-methyl-;209391-60-6;DTXSID90466717

Suppliers and Price of Benzene, 1-[(1-chloro-2,2-diphenylethenyl)sulfinyl]-4-methyl-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Total 1 raw suppliers

Chemical Property of Benzene, 1-[(1-chloro-2,2-diphenylethenyl)sulfinyl]-4-methyl-

Chemical Property:

XLogP3:6.2
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:4
Exact Mass:352.0688640
Heavy Atom Count:24
Complexity:433

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CC1=CC=C(C=C1)S(=O)C(=C(C2=CC=CC=C2)C3=CC=CC=C3)Cl

Technology Process of Benzene, 1-[(1-chloro-2,2-diphenylethenyl)sulfinyl]-4-methyl-

There total 5 articles about Benzene, 1-[(1-chloro-2,2-diphenylethenyl)sulfinyl]-4-methyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 209391-96-8
Acetic acid 2-chloro-1,1-diphenyl-2-(toluene-4-sulfinyl)-ethyl ester

: 209391-60-6
[2-chloro-2-(p-tolylsulfinyl)ethene-1,1-diyl]dibenzene

Guidance literature:: With sodium hydride; 1,8-diazabicyclo[5.4.0]undec-7-ene; In tetrahydrofuran; for 3.5h; Ambient temperature;
DOI:10.1016/S0040-4020(98)00243-9

Reference yield:

: 209391-91-3
2-Chloro-1,1-diphenyl-2-(toluene-4-sulfinyl)-ethanol

: 209391-60-6
[2-chloro-2-(p-tolylsulfinyl)ethene-1,1-diyl]dibenzene

Guidance literature:: Multi-step reaction with 2 steps

1: 89 percent / DMAP, Py / 16 h / Ambient temperature

2: 78 percent / NaH, DBU / tetrahydrofuran / 3.5 h / Ambient temperature

With pyridine; dmap; sodium hydride; 1,8-diazabicyclo[5.4.0]undec-7-ene; In tetrahydrofuran;
DOI:10.1016/S0040-4020(98)00243-9

Reference yield:

: 119-61-9
benzophenone

: 209391-60-6
[2-chloro-2-(p-tolylsulfinyl)ethene-1,1-diyl]dibenzene

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) LDA / 1.) THF, -78 deg C, 10 min, 2.) THF, -78 deg C, 10 min.

2: 89 percent / DMAP, Py / 16 h / Ambient temperature

3: 78 percent / NaH, DBU / tetrahydrofuran / 3.5 h / Ambient temperature

With pyridine; dmap; sodium hydride; 1,8-diazabicyclo[5.4.0]undec-7-ene; lithium diisopropyl amide; In tetrahydrofuran;
DOI:10.1016/S0040-4020(98)00243-9