Ruthenium, tetrakis(benzonitrile)dichloro-

Base Information

Chemical Name:Ruthenium, tetrakis(benzonitrile)dichloro-
CAS No.:21503-87-7
Molecular Formula:C₂₈H₂₀Cl₂N₄Ru
Molecular Weight:584.47
Hs Code.:
Mol file:21503-87-7.mol

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Chemical Property of Ruthenium, tetrakis(benzonitrile)dichloro-

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Technology Process of Ruthenium, tetrakis(benzonitrile)dichloro-

There total 3 articles about Ruthenium, tetrakis(benzonitrile)dichloro- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 14898-67-0
ruthenium(III) chloride trihydrate

: 100-47-0
benzonitrile

: 21503-87-7,51014-03-0
trans-{RuCl₂(C₆H₅CN)4}

Guidance literature:: With hydrogen; platinum(IV) oxide; In methanol; addn. of C6H5CN to soln. of RuCl3*3H2O; refluxing for 3h under N2; cooling; agitating with PtO2 under H2-atmosphere; evapn. in vac.; washing (ether); dissolving in warm CH2Cl2; filtration;careful addn. of ether to filtrate; pptn.;

Reference yield: 89.0%

: 14898-67-0
ruthenium trichloride hydrate

: 100-47-0
benzonitrile

: 21503-87-7,51014-03-0
trans-{RuCl₂(C₆H₅CN)4}

Guidance literature:: In methanol; benzonitrile; the educt was heated in MeOH/PhCN at 80 °C for 4 h, then at 120 °C for 48 h (until the color has changed from red orange to yellow);; the ppt. was collected, addn. of diethyl ether to the supernatant soln. yielded a second fraction; elem.anal.;;
DOI:10.1039/DT9910002401

Reference yield:

: mer-{N(C₄H₉)4}{RuCl₃(C₆H₅CN)3}

: 100-47-0
benzonitrile

: 21503-87-7,51014-03-0
trans-{RuCl₂(C₆H₅CN)4}

Guidance literature:: In dichloromethane; benzonitrile; Electrochem. Process; (RuCl3(C6H5CN)3)(1-), produced electrochemically, was further substituted at room temp. in 10% PhCN - 90% CH2Cl2 soln.; elem.anal.;
DOI:10.1039/DT9910002401