benzylthiodimesitylborane

Base Information

Chemical Name:benzylthiodimesitylborane
CAS No.:77657-17-1
Molecular Formula:C₂₅H₂₉BS
Molecular Weight:372.382
Hs Code.:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of benzylthiodimesitylborane

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Technology Process of benzylthiodimesitylborane

There total 1 articles about benzylthiodimesitylborane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 436-59-9
dimesitylfluoroborane

: 925-90-6
ethylmagnesium bromide

: 100-53-8
phenylmethanethiol

: 77657-17-1
benzylthiodimesitylborane

Guidance literature:: In diethyl ether; byproducts: C2H6, MgBrF; under N2 to a soln. of EtMgBr in ether an ether soln. of thiol was added at 0°C, stirred for 2 h at room temp., a soln. of B-compound inether was added at room temp., stirred overnight; filtered through anhyd. MgSO4, evapd., triturated with pentane/ether;
DOI:10.1016/S0022-328X(00)84580-5