Neopentyloxybenzene

Base Information

• Chemical Name: Neopentyloxybenzene
• CAS No.: 2189-88-0
• Molecular Formula: C11H16O
• Molecular Weight: 164.247
• Mol file: 2189-88-0.mol

Synonyms:Neopentyl-phenylaether;neopentyl phenyl ether;Phenoxyneopentan;Neopentylphenylaether;2-Methyl-2-phenyoxymethyl-propan;Neopentyloxybenzol;

Chemical Property of Neopentyloxybenzene

Chemical Property:

• PSA: 9.23000
• LogP: 3.11150

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Neopentyloxybenzene

There total 5 articles about Neopentyloxybenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

neopentyl iodide (15501-33-4) + phenol (108-95-2,27073-41-2) → 1-phenoxy-2,2-dimethylpropane (2189-88-0)

Guidance literature:

With CsCO₃; In diethylene glycol dimethyl ether; at 150 - 160 ℃; for 12h; reduced pressure;

Reference yield: 75.0%

neopentyloxy-tris(dimethylamino)phosphonium hexafluorophosphate (54739-01-4) + phenol (108-95-2,27073-41-2) → 1-phenoxy-2,2-dimethylpropane (2189-88-0)

Guidance literature:

With potassium hydroxide; In N,N-dimethyl-formamide; for 15h; Heating;

DOI:10.1016/S0040-4020(01)81713-0

Reference yield: 62.0%

2,2-dimethyl-propanol-1 (75-84-3) + tetraphenyl-bismuth trifluoroacetate (83566-43-2) → trifluoroacetic acid, 2,2-dimethylpropyl ester (7556-79-8) + 1-phenoxy-2,2-dimethylpropane (2189-88-0)

Guidance literature:

In benzene-d6; 25 h reflux (Ar); monitored by (1)H NMR;

DOI:10.1039/P19870000251

upstream raw materials:

2-Phenoxymethyl-2-methyl-propan-1,3-diyl-bis-

neopentyloxy-tris(dimethylamino)phosphonium hexafluorophosphate

phenol

2,2-dimethyl-propanol-1

Downstream raw materials:

4-(2,2-dimethylpropyloxy)nitrobenzene

2-methyl-but-2-ene

1,1-dimethylcyclopropane

2-Methyl-1-butene

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