TERT-BUTYL THIOMORPHOLINE-4-CARBOXYLATE

Base Information

• Chemical Name: TERT-BUTYL THIOMORPHOLINE-4-CARBOXYLATE
• CAS No.: 220655-09-4
• Molecular Formula: C9H17NO2S
• Molecular Weight: 203.305
• Hs Code.: 2934999090
• Mol file: 220655-09-4.mol

Synonyms:N-Boc-thiomorpholine;N-tert-butoxycarbonyl-thiomorpholine;N-tert-butyloxycarbonyl thiomorpholine;

Chemical Property of TERT-BUTYL THIOMORPHOLINE-4-CARBOXYLATE

Chemical Property:

• PSA: 54.84000
• LogP: 1.90820

Purity/Quality:

97% ^*data from raw suppliers

tert-Butylthiomorpholine-4-carboxylate 95+% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Uses: tert-Butyl thiomorpholine-4-carboxylate is used as a reactant in the preparation of aromatic heterocyclic ureas as antiinflammatory agents.

Technology Process of TERT-BUTYL THIOMORPHOLINE-4-CARBOXYLATE

There total 2 articles about TERT-BUTYL THIOMORPHOLINE-4-CARBOXYLATE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

Thiomorpholin (123-90-0) + di-tert-butyl dicarbonate (24424-99-5) → tert-butyl thiomorpholine-4-carboxylate (220655-09-4)

Guidance literature:

With triethylamine; In dichloromethane;

Reference yield:

Thiomorpholin (123-90-0) + di-tert-butyl dicarbonate (24424-99-5) → tert-butyl thiomorpholine-4-carboxylate (220655-09-4) + BzlSO2-norLeu(cyclo)-Gly-LysΨ[COCO]-(1,1-dioxo)thiomorpholin4-yl

Guidance literature:

With triethylamine; In methanol; ethyl acetate;

Reference yield: 99.0%

tert-butyl thiomorpholine-4-carboxylate (220655-09-4) → tert-butyl thiomorpholine-4-carboxylate-1-oxide (278788-74-2)

Guidance literature:

With sodium periodate; In 1,4-dioxane; methanol; water; at 0 ℃; for 5.5h;

upstream raw materials:

Thiomorpholin

di-tert-butyl dicarbonate

Downstream raw materials:

tert-butyl thiomorpholine-4-carboxylic acid-1,1-dioxide

tert-butyl thiomorpholine-4-carboxylate-1-oxide

thiomorpholine 1,1-dioxide

N-(tert-butoxycarbonyl)-3-pyrroline

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