2H-Thiopyran, tetrahydro-4-phenyl-

Base Information

Chemical Name:2H-Thiopyran, tetrahydro-4-phenyl-
CAS No.:22398-05-6
Molecular Formula:C11H14S
Molecular Weight:178.298
Hs Code.:

Synonyms:

Suppliers and Price of 2H-Thiopyran, tetrahydro-4-phenyl-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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Total 4 raw suppliers

Chemical Property of 2H-Thiopyran, tetrahydro-4-phenyl-

Chemical Property:

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 2H-Thiopyran, tetrahydro-4-phenyl-

There total 4 articles about 2H-Thiopyran, tetrahydro-4-phenyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.0%

: Li[(phenyl)(butyl)B((pinacol)(-2H))]

: 281204-90-8
4-iodotetrahydro-2H-thiopyran

: 22398-05-6
4-phenylthiane

Guidance literature:: With tetrakis(actonitrile)copper(I) hexafluorophosphate; 1-methyl-1-phenylethyl triethylsilyl peroxide; triethylamine; In tetrahydrofuran; dimethyl sulfoxide; at 20 ℃; for 1h; Sealed tube; Inert atmosphere;
DOI:10.1021/jacs.1c12649

Reference yield:

: 24388-23-6
2-phenyl-4,4,5,5-tetramethyl-1,3,2-dioxoborole

: 22398-05-6
4-phenylthiane

Guidance literature:: Multi-step reaction with 2 steps

1: tetrahydrofuran / 1 h / -78 - 20 °C / Inert atmosphere; Sealed tube

2: triethylamine; 1-methyl-1-phenylethyl triethylsilyl peroxide; tetrakis(actonitrile)copper(I) hexafluorophosphate / tetrahydrofuran; dimethyl sulfoxide / 1 h / 20 °C / Sealed tube; Inert atmosphere

With tetrakis(actonitrile)copper(I) hexafluorophosphate; 1-methyl-1-phenylethyl triethylsilyl peroxide; triethylamine; In tetrahydrofuran; dimethyl sulfoxide; 2: |Suzuki-Miyaura Coupling;
DOI:10.1021/jacs.1c12649

Reference yield:

: 29683-23-6
tetrahydrothiopyran-4-ol

: 22398-05-6
4-phenylthiane

Guidance literature:: Multi-step reaction with 2 steps

1: iodine; triphenylphosphine; 1H-imidazole / dichloromethane / 16 h / 0 - 20 °C / Inert atmosphere

2: triethylamine; 1-methyl-1-phenylethyl triethylsilyl peroxide; tetrakis(actonitrile)copper(I) hexafluorophosphate / tetrahydrofuran; dimethyl sulfoxide / 1 h / 20 °C / Sealed tube; Inert atmosphere

With 1H-imidazole; tetrakis(actonitrile)copper(I) hexafluorophosphate; 1-methyl-1-phenylethyl triethylsilyl peroxide; iodine; triethylamine; triphenylphosphine; In tetrahydrofuran; dichloromethane; dimethyl sulfoxide; 1: |Appel Halogenation / 2: |Suzuki-Miyaura Coupling;
DOI:10.1021/jacs.1c12649