Ethanone,2-(2,4-dimethoxyphenyl)-1-(2-hydroxy-4,6-dimethoxyphenyl)-

Base Information

• Chemical Name: Ethanone,2-(2,4-dimethoxyphenyl)-1-(2-hydroxy-4,6-dimethoxyphenyl)-
• CAS No.: 39604-69-8
• Molecular Formula: C18H20 O6
• Molecular Weight: 332.353
• Hs Code.: 2914509090
• Mol file: 39604-69-8.mol

Synonyms:Acetophenone,2-(2,4-dimethoxyphenyl)-2'-hydroxy-4',6'-dimethoxy- (6CI,7CI); 2-(2,4-Dimethoxyphenyl)-1-(2-hydroxy-4,6-dimethoxyphenyl)ethanone;2-Hydroxy-4,6-dimethoxyphenyl 2,4-dimethoxybenzyl ketone; Albizoin

Chemical Property of Ethanone,2-(2,4-dimethoxyphenyl)-1-(2-hydroxy-4,6-dimethoxyphenyl)-

Chemical Property:

• Melting Point: 139°C
• PSA: 74.22000
• LogP: 2.85200

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Ethanone,2-(2,4-dimethoxyphenyl)-1-(2-hydroxy-4,6-dimethoxyphenyl)-

There total 9 articles about Ethanone,2-(2,4-dimethoxyphenyl)-1-(2-hydroxy-4,6-dimethoxyphenyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

1,2,3-trimethoxybenzene (621-23-8) + 2,4-dimethoxyphenylacetic acid (6496-89-5) → 1-(2'-hydroxy-4',6'-dimethoxyphenyl)-2-(2,4-dimethoxyphenyl)ethanone (39604-69-8)

Guidance literature:

With boron trifluoride diethyl etherate; at 70 ℃; Inert atmosphere;

DOI:10.1016/j.tet.2019.130589

Reference yield: 68.0%

2,4,6,2',4'-pentamethoxy-deoxybenzoin (521291-07-6) → 1-(2'-hydroxy-4',6'-dimethoxyphenyl)-2-(2,4-dimethoxyphenyl)ethanone (39604-69-8)

Guidance literature:

With aluminium trichloride; In chloroform;

DOI:10.1016/S0960-894X(03)00394-9

Reference yield:

2-(2,4-dimethoxyphenyl)-1-(2,4,6-trihydroxyphenyl)-ethanone (65568-08-3) + dimethyl sulfate (77-78-1) → 1-(2'-hydroxy-4',6'-dimethoxyphenyl)-2-(2,4-dimethoxyphenyl)ethanone (39604-69-8)

Guidance literature:

upstream raw materials:

5,7,2',4'-tetramethoxyisoflavone

3-(2,4-dimethoxy-phenyl)-5,7-dimethoxy-chroman-4-one

2,4,6,2',4'-pentamethoxy-deoxybenzoin

2-(2,4-dimethoxyphenyl)-1-(2,4,6-trihydroxyphenyl)-ethanone

Downstream raw materials:

3-(2',4'-dimethoxyphenyl)-4-hydroxy-5,7-dimethoxy-2H-1-benzopyrane-2-one

2,4,6,2',4'-pentamethoxy-deoxybenzoin

5,7,2',4'-tetramethoxyisoflavone

1-(2,4-Dimethoxy-phenyl)-2-(2-hydroxy-4,6-dimethoxy-phenyl)-ethane-1,2-dione