(4E)-4-{[2-(5,6-diphenyl-1,2,4-triazin-3-yl)hydrazino]methylidene}-3-hydroxycyclohexa-2,5-dien-1-one

Base Information

• Chemical Name: (4E)-4-{[2-(5,6-diphenyl-1,2,4-triazin-3-yl)hydrazino]methylidene}-3-hydroxycyclohexa-2,5-dien-1-one
• CAS No.: 5470-45-1
• Molecular Formula: C₁₆H₂₆I₂NO₃P
• Molecular Weight: 565.17
• Mol file: 5470-45-1.mol

Synonyms:Phosphonicacid, [p-[bis(2-iodoethyl)amino]-a-methylbenzyl]-, diethyl ester (6CI); NSC 27407

Chemical Property of (4E)-4-{[2-(5,6-diphenyl-1,2,4-triazin-3-yl)hydrazino]methylidene}-3-hydroxycyclohexa-2,5-dien-1-one

Chemical Property:

• Vapor Pressure: 4.45E-14mmHg at 25°C
• Boiling Point: 575.4°C at 760 mmHg
• Flash Point: 301.8°C
• Density: 1.429g/cm³

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of (4E)-4-{[2-(5,6-diphenyl-1,2,4-triazin-3-yl)hydrazino]methylidene}-3-hydroxycyclohexa-2,5-dien-1-one

There total 5 articles about (4E)-4-{[2-(5,6-diphenyl-1,2,4-triazin-3-yl)hydrazino]methylidene}-3-hydroxycyclohexa-2,5-dien-1-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

diethyl (1-phenylethyl)phosphonate (33973-48-7) → (1-{4-[bis-(2-iodo-ethyl)-amino]-phenyl}-ethyl)-phosphonic acid diethyl ester (5470-45-1)

Guidance literature:

Multi-step reaction with 3 steps

1: H₂SO₄; HNO₃

2: platinum / Hydrogenation

3: ueber mehrere Stufen

With sulfuric acid; nitric acid; platinum;

DOI:10.1021/ja01521a029

Reference yield:

diethyl 1-(4-nitrophenyl)ethylphosphonate (115050-50-5) → (1-{4-[bis-(2-iodo-ethyl)-amino]-phenyl}-ethyl)-phosphonic acid diethyl ester (5470-45-1)

Guidance literature:

Multi-step reaction with 2 steps

1: platinum / Hydrogenation

2: ueber mehrere Stufen

With platinum;

DOI:10.1021/ja01521a029

Reference yield:

(1-bromoethyl)benzne (585-71-7,38661-81-3) → (1-{4-[bis-(2-iodo-ethyl)-amino]-phenyl}-ethyl)-phosphonic acid diethyl ester (5470-45-1)

Guidance literature:

Multi-step reaction with 4 steps

2: H₂SO₄; HNO₃

3: platinum / Hydrogenation

4: ueber mehrere Stufen

With sulfuric acid; nitric acid; platinum;

DOI:10.1021/ja01521a029

upstream raw materials:

[1-(4-amino-phenyl)-ethyl]-phosphonic acid diethyl ester

oxirane

diethyl (1-phenylethyl)phosphonate

diethyl 1-(4-nitrophenyl)ethylphosphonate