1-Methyl-2,4,6-triphenylpyridinium tetrafluoroborate

Base Information

• Chemical Name: 1-Methyl-2,4,6-triphenylpyridinium tetrafluoroborate
• CAS No.: 2355-56-8
• Molecular Formula: C24H20N.BF4
• Molecular Weight: 409.234
• European Community (EC) Number: 651-783-6
• ChEMBL ID: CHEMBL578751
• Mol file: 2355-56-8.mol

Synonyms:2355-56-8;1-METHYL-2,4,6-TRIPHENYLPYRIDINIUMTETRAFLUOROBORATE;GNF-Pf-1833;1-Methyl-2,4,6-triphenylpyridinium tetrafluoroborate;CHEMBL578751;AKOS024427112;FT-0608045;1-Methyl-2,4,6-triphenylpyridin-1-ium tetrafluoroborate

Chemical Property of 1-Methyl-2,4,6-triphenylpyridinium tetrafluoroborate

Chemical Property:

• PSA: 3.88000
• LogP: 6.81210
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 5
• Rotatable Bond Count: 3
• Exact Mass: 409.1624925
• Heavy Atom Count: 30
• Complexity: 378

Purity/Quality:

98%Min ^*data from raw suppliers

1-METHYL-2,4,6-TRIPHENYLPYRIDINIUM TETRAFLUOROBORATE AldrichCPR ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

• Canonical SMILES: [B-](F)(F)(F)F.C[N+]1=C(C=C(C=C1C2=CC=CC=C2)C3=CC=CC=C3)C4=CC=CC=C4

Technology Process of 1-Methyl-2,4,6-triphenylpyridinium tetrafluoroborate

There total 2 articles about 1-Methyl-2,4,6-triphenylpyridinium tetrafluoroborate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

2,4,6-triphenylpyrylium tetrafluoroborate (448-61-3) + methylamine (74-89-5) → 1N-methyl-2,4,6-triphenylpyridinium tetrafluoroborate (2355-56-8)

Guidance literature:

With sodium acetate; In ethanol; at 90 ℃; for 24h; Inert atmosphere;

DOI:10.1021/ja108668h

Reference yield: 40.0%

2,4,6-triphenylpyrylium tetrafluoroborate (448-61-3) + methylamine (74-89-5) → 2,4,6-triphenylpyridine (580-35-8) + 1N-methyl-2,4,6-triphenylpyridinium tetrafluoroborate (2355-56-8) + 2,4,6-triphenyl-N-methylpiperidine (95349-87-4)

Guidance literature:

With hydrogen; nickel ruthenium; In methanol; at 100 ℃; under 7598.1 Torr; Product distribution;

DOI:10.1007/BF00505960

Reference yield: 100.0%

1N-methyl-2,4,6-triphenylpyridinium tetrafluoroborate (2355-56-8) → 1,4-dihydro-2,4,6-triphenyl-N-methyl-pyridine

Guidance literature:

With sodium amalgam; In ethanol;

DOI:10.1002/poc.532

upstream raw materials:

2,4,6-triphenylpyrylium tetrafluoroborate

methylamine

Downstream raw materials:

N,N,S-trimethyldithiocarbamate

N-methylphthalimide

N-methylbenzenesulfonanilide

2-Methyl-2-nitropropane

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