3-(Prop-1-en-2-yl)aniline

Base Information

Chemical Name:3-(Prop-1-en-2-yl)aniline
CAS No.:23809-98-5
Molecular Formula:C9H11N
Molecular Weight:133.193
Hs Code.:
European Community (EC) Number:868-141-8
Mol file:23809-98-5.mol

Synonyms:3-(prop-1-en-2-yl)aniline;23809-98-5;3-prop-1-en-2-ylaniline;2-(3-aminophenyl)propene;SCHEMBL771139;AKOS006364302;EN300-754548;Z1203585283

Suppliers and Price of 3-(Prop-1-en-2-yl)aniline

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 1 raw suppliers

Chemical Property of 3-(Prop-1-en-2-yl)aniline

Chemical Property:

XLogP3:2.4
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:1
Exact Mass:133.089149355
Heavy Atom Count:10
Complexity:129

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CC(=C)C1=CC(=CC=C1)N

Technology Process of 3-(Prop-1-en-2-yl)aniline

There total 3 articles about 3-(Prop-1-en-2-yl)aniline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 1779-49-3
Methyltriphenylphosphonium bromide

: 99-03-6
1-(3-aminophenyl)ethanone

: 23809-98-5
3-(prop-1-en-2-yl)aniline

Guidance literature:: Methyltriphenylphosphonium bromide; With potassium tert-butylate; In tetrahydrofuran; at 0 - 20 ℃; for 0.5h; Schlenk technique; Inert atmosphere;

1-(3-aminophenyl)ethanone; In tetrahydrofuran; at 0 - 20 ℃; Schlenk technique; Inert atmosphere;
DOI:10.1002/chem.201606026

Reference yield: 59.0%

: 64416-49-5
3-(1-methylethenyl)nitrobenzene

: 23809-98-5
3-(prop-1-en-2-yl)aniline

Guidance literature:: With iron; acetic acid; In ethanol; at 100 ℃; for 2h; Inert atmosphere;
DOI:10.1016/j.bmc.2016.07.012

Reference yield:

: 121-89-1
3-Nitroacetophenone

: 23809-98-5
3-(prop-1-en-2-yl)aniline

Guidance literature:: Multi-step reaction with 2 steps

1: n-butyllithium / tetrahydrofuran; hexane / 1 h / -5 - 20 °C / Inert atmosphere

2: iron; acetic acid / ethanol / 2 h / 100 °C / Inert atmosphere

With n-butyllithium; iron; acetic acid; In tetrahydrofuran; ethanol; hexane;
DOI:10.1016/j.bmc.2016.07.012