Technology Process of 2-Quinolinecarboxylic acid, 5,6,7,8-tetrahydro-8-oxo-
There total 5 articles about 2-Quinolinecarboxylic acid, 5,6,7,8-tetrahydro-8-oxo- which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
formic acid; dihydrogen peroxide;
In
water;
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: 98 percent / H2; TFA / 10percent Pd/C / 60 h / 20 °C
2.1: 79 percent / Ac2O / 120 h / 150 - 160 °C
3.1: O3 / CH2Cl2; methanol / -77 °C
3.2: 89 percent / Me2S / CH2Cl2; methanol / -77 - 20 °C
4.1: 88 percent / 30percent aq. H2O2; HCO2H / 3 h / 20 °C
With
formic acid; hydrogen; acetic anhydride; ozone; trifluoroacetic acid;
10percent Pd/C;
In
methanol; dichloromethane;
DOI:10.1021/ja0273694
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: H2; CF3COOH / 10 percent Pd/C / 20 °C
2.1: Ac2O / 150 - 160 °C
3.1: O3; O2 / CH2Cl2; methanol / -77 °C
3.2: Me2S / CH2Cl2; methanol / -77 - 20 °C
4.1: CrO3; H2SO4 / acetone / 20 °C
With
chromium(VI) oxide; sulfuric acid; hydrogen; oxygen; acetic anhydride; ozone; trifluoroacetic acid;
palladium on activated charcoal;
In
methanol; dichloromethane; acetone;
1.1: Catalytic hydrogenation / 2.1: Condensation / 3.1: Oxidation / 3.2: Decomposition / 4.1: Oxidation;
DOI:10.1002/(SICI)1521-3773(19990903)38:17<2543::AID-ANIE2543>3.0.CO;2-9