Technology Process of 1,3-Benzenedicarboxylic acid, 4-[[(trifluoromethyl)sulfonyl]oxy]-,
3-(phenylmethyl) ester
There total 4 articles about 1,3-Benzenedicarboxylic acid, 4-[[(trifluoromethyl)sulfonyl]oxy]-,
3-(phenylmethyl) ester which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
sodium chlorite; sodium dihydrogenphosphate; 2-methyl-but-2-ene;
In
water; acetonitrile; tert-butyl alcohol;
at 20 ℃;
Inert atmosphere;
Cooling with ice;
DOI:10.1016/j.bmc.2009.04.013
- Guidance literature:
-
Multi-step reaction with 2 steps
1: pyridine / CH2Cl2 / 0.5 h / 20 °C
2: NaH2PO4*H2O; 2-methyl-2-butene; sodium chlorite / 2-methyl-propan-2-ol; H2O; acetonitrile / 1 h / 20 °C
With
pyridine; sodium chlorite; sodium dihydrogenphosphate; 2-methyl-but-2-ene;
In
dichloromethane; water; acetonitrile; tert-butyl alcohol;
DOI:10.1016/j.bmc.2006.08.010
- Guidance literature:
-
Multi-step reaction with 3 steps
1: sodium hydrogencarbonate / N,N-dimethyl-formamide
2: pyridine / -10 °C
3: sodium chlorite; sodium dihydrogen phosphate monohydrate; 2-methyl-but-2-ene / tert-butyl alcohol; acetonitrile; water
With
pyridine; sodium chlorite; sodium dihydrogen phosphate monohydrate; 2-methyl-but-2-ene; sodium hydrogencarbonate;
In
water; N,N-dimethyl-formamide; acetonitrile; tert-butyl alcohol;
DOI:10.1016/j.bmcl.2013.06.028
