Benzoic acid, 2-cycloheptylidenehydrazide

Base Information

• Chemical Name: Benzoic acid, 2-cycloheptylidenehydrazide
• CAS No.: 24214-80-0
• Molecular Formula: C14H18N2O
• Molecular Weight: 230.31
• DSSTox Substance ID: DTXSID801272757

Synonyms:SCHEMBL20621742;DTXSID801272757;AKOS003851036;Benzoic acid, 2-cycloheptylidenehydrazide;24214-80-0

Chemical Property of Benzoic acid, 2-cycloheptylidenehydrazide

Chemical Property:

• XLogP3: 2.9
• Hydrogen Bond Donor Count: 1
• Hydrogen Bond Acceptor Count: 2
• Rotatable Bond Count: 2
• Exact Mass: 230.141913202
• Heavy Atom Count: 17
• Complexity: 270

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

• Canonical SMILES: C1CCCC(=NNC(=O)C2=CC=CC=C2)CC1

Technology Process of Benzoic acid, 2-cycloheptylidenehydrazide

There total 1 articles about Benzoic acid, 2-cycloheptylidenehydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

→ cycloheptanone benzoylhydrazone (24214-80-0)

Guidance literature:

Benzoesaeurehydrazid, A., Cycloheptanon, Sieden, 2 h;

Reference yield: 48.0%

cycloheptanone benzoylhydrazone (24214-80-0) + 1-chloro-1-[(4-chlorophenyl)hydrazono]propanone (18247-78-4,1338563-31-7) → 3-acetyl-4-benzoylamino-1-(4'-chlorophenyl)-1,2,4-triazaspiro[4.6]undec-2-ene

Guidance literature:

With triethylamine; In tetrahydrofuran; at 0 - 20 ℃;

DOI:10.1081/SCC-120015707

Reference yield:

cycloheptanone benzoylhydrazone (24214-80-0) + 5-chloro-2-aminobenzophenone (719-59-5) → 2-chloro-11-phenyl-7,8,9,10-tetrahydro-6H-cyclohepta[b]quinoline (116690-73-4)

Guidance literature:

Yield given. Multistep reaction;

Downstream raw materials:

2-chloro-11-phenyl-7,8,9,10-tetrahydro-6H-cyclohepta[b]quinoline

11-phenyl-7,8,9,10-tetrahydro-6H-cyclohepta[b]quinoline

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