1,3-Benzodioxol-4-ol, 5-(methoxymethoxy)-

Base Information

Chemical Name:1,3-Benzodioxol-4-ol, 5-(methoxymethoxy)-
CAS No.:244126-41-8
Molecular Formula:C9H10O5
Molecular Weight:198.175
Hs Code.:
DSSTox Substance ID:DTXSID40465058
Nikkaji Number:J1.752.900E
Wikidata:Q82290723
Mol file:244126-41-8.mol

Synonyms:244126-41-8;1,3-Benzodioxol-4-ol, 5-(methoxymethoxy)-;5-(Methoxymethoxy)benzo[d][1,3]dioxol-4-ol;5-(methoxymethoxy)-1,3-benzodioxol-4-ol;SCHEMBL1755311;DTXSID40465058;CS-M2924;AKOS030616818;CS-14840;C12805;5-(METHOXYMETHOXY)-2H-1,3-BENZODIOXOL-4-OL

Suppliers and Price of 1,3-Benzodioxol-4-ol, 5-(methoxymethoxy)-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 6 raw suppliers

Chemical Property of 1,3-Benzodioxol-4-ol, 5-(methoxymethoxy)-

Chemical Property:

XLogP3:1.3
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:5
Rotatable Bond Count:3
Exact Mass:198.05282342
Heavy Atom Count:14
Complexity:186

Purity/Quality:: 97% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:COCOC1=C(C2=C(C=C1)OCO2)O

Technology Process of 1,3-Benzodioxol-4-ol, 5-(methoxymethoxy)-

There total 5 articles about 1,3-Benzodioxol-4-ol, 5-(methoxymethoxy)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 111726-43-3
3,4-(methylenedioxy)phenyl methoxymethyl ether

: 244126-41-8
4-hydroxy-5-(methoxymethoxy)-1,3-benzodioxole

Guidance literature:: 3,4-(methylenedioxy)phenyl methoxymethyl ether; With n-butyllithium; Trimethyl borate; In tetrahydrofuran;

With dihydrogen peroxide; acetic acid; at 0 - 20 ℃;
DOI:10.1021/ja0571794

Reference yield: 59.0%

: 316800-43-8
formic acid 5-methoxymethoxy-benzo[1,3]dioxol-4-yl ester

: 244126-41-8
4-hydroxy-5-(methoxymethoxy)-1,3-benzodioxole

Guidance literature:: With sodium hydroxide; In tetrahydrofuran; at 20 ℃; for 4h;
DOI:10.1139/v00-138

Reference yield:

: 533-31-3
Sesamol

: 244126-41-8
4-hydroxy-5-(methoxymethoxy)-1,3-benzodioxole

Guidance literature:: Multi-step reaction with 2 steps

1.1: 96 percent / NaH / diethyl ether; dimethylformamide / 0 - 20 °C

2.1: n-BuLi; B(OMe)3 / tetrahydrofuran

2.2: 95 percent / AcOH; H₂O₂ / 0 - 20 °C

With n-butyllithium; Trimethyl borate; sodium hydride; In tetrahydrofuran; diethyl ether; N,N-dimethyl-formamide;
DOI:10.1021/ja0571794