Os₃(CO)11(1,3-bis(diphenylphosphino)propane monoxide)(GaCl₃)

Base Information

• Chemical Name: Os₃(CO)11(1,3-bis(diphenylphosphino)propane monoxide)(GaCl₃)
• CAS No.: 1392301-03-9
• Molecular Formula: C₃₈H₂₆Cl₃GaO₁₂Os₃P₂
• Molecular Weight: 1483.25
• Mol file: 1392301-03-9.mol

Synonyms:

Chemical Property of Os₃(CO)11(1,3-bis(diphenylphosphino)propane monoxide)(GaCl₃)

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of Os₃(CO)11(1,3-bis(diphenylphosphino)propane monoxide)(GaCl₃)

There total 1 articles about Os₃(CO)11(1,3-bis(diphenylphosphino)propane monoxide)(GaCl₃) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

Os3(CO)11(1,3-bis(diphenylphosphino)propane monoxide) (1392300-98-9) + Gallium trichloride (13450-90-3) → Os3(CO)11(1,3-bis(diphenylphosphino)propane monoxide)(GaCl3) (1392301-03-9)

Guidance literature:

In toluene; under Ar, Schlenk techniques; metal cluster dissolved in toluene and cooled in dry ice/iPrOH bath, GaCl3 added, after 1 h warmed to room temp.; solvents removed in vac., dissolved in CH2Cl2, SiO2 column (CH2Cl2/n-hexane/acetone = 40/40/15), heptane added, solvents removed in vac.; elem. anal., unremovable admixture of Ga compds.;

DOI:10.1016/j.jorganchem.2012.03.003

upstream raw materials:

Os₃(CO)11(1,3-bis(diphenylphosphino)propane monoxide)

Gallium trichloride