2-[4-(Dimethylamino)phenyl]-1,3-dithiane

Base Information

• Chemical Name: 2-[4-(Dimethylamino)phenyl]-1,3-dithiane
• CAS No.: 24588-75-8
• Molecular Formula: C12H17NS2
• Molecular Weight: 239.406
• Hs Code.: 2934999090
• Mol file: 24588-75-8.mol

Synonyms:(4-[1,3]dithian-2-ylphenyl)dimethylamine;2-(4-N,N-dimethylaminophenyl)-1,3-dithiane;4-(1,3-dithian-2-yl)-N,N-dimethylbenzenamine;2-[4-(dimethylamino)phenyl]-1,3-dithiane;2-<4-(Dimethylamino)phenyl>-1,3-dithian;4-(N,N'-dimethylamino)phenyl-1,3-dithiane;

Chemical Property of 2-[4-(Dimethylamino)phenyl]-1,3-dithiane

Chemical Property:

• Vapor Pressure: 2.84E-06mmHg at 25°C
• Boiling Point: 389.5oC at 760 mmHg
• Flash Point: 189.4oC
• PSA: 53.84000
• Density: 1.153g/cm3
• LogP: 3.62130

Purity/Quality:

97% ^*data from raw suppliers

2-[4-(DIMETHYLAMINO)PHENYL]-1,3-DITHIANE 95.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2-[4-(Dimethylamino)phenyl]-1,3-dithiane

There total 8 articles about 2-[4-(Dimethylamino)phenyl]-1,3-dithiane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

1.3-propanedithiol (109-80-8) + 4-dimethylamino-benzaldehyde (100-10-7) → 4-(N,N'-dimethylamino)phenyl-1,3-dithiane (24588-75-8)

Guidance literature:

at 20 ℃;

DOI:10.24820/ARK.5550190.P011.476

Reference yield: 97.0%

4-dimethylamino-benzaldehyde (100-10-7) + 3‐(1,3-dithiane-2-yl)pentane-2,4-dione (55727-23-6) → 4-(N,N'-dimethylamino)phenyl-1,3-dithiane (24588-75-8)

Guidance literature:

With para-dodecylbenzenesulfonic acid; In water; for 2.1h; Heating;

DOI:10.1021/jo050271y

Reference yield: 93.0%

4-dimethylamino-benzaldehyde (100-10-7) + 2-(1,3-dithian-2-ylidene)malonic acid (461024-59-9) → 4-(N,N'-dimethylamino)phenyl-1,3-dithiane (24588-75-8)

Guidance literature:

With para-dodecylbenzenesulfonic acid; In water; for 2h; Heating;

DOI:10.1080/00397910601163984

upstream raw materials:

1,3-dithian-2-yl tetrafluoroborate

N,N-dimethyl-aniline

4-dimethylamino-benzaldehyde

2,4-dichloro-3-(1,3-propylenedithio-methylene)-penta-1,4-diene

Downstream raw materials:

[2-(4-Dimethylamino-phenyl)-[1,3]dithian-2-yl]-phenyl-methanone oxime

2-(2-bromobenzyl)-2-[4-(dimethylamino)phenyl]-1,3-dithiane

1-(2-Chloro-phenyl)-2-(4-dimethylamino-phenyl)-ethane-1,2-dione

4-N,N-dimethylphenyl triethylsilyl ketone