4,4',4''-Methanetriyltris(N,N,3-trimethylaniline)

Base Information

• Chemical Name: 4,4',4''-Methanetriyltris(N,N,3-trimethylaniline)
• CAS No.: 24619-07-6
• Molecular Formula: C28H37N3
• DSSTox Substance ID: DTXSID30562262
• Wikidata: Q82446345
• Mol file: 24619-07-6.mol

Synonyms:24619-07-6;4,4',4''-Methanetriyltris(N,N,3-trimethylaniline);SCHEMBL3193700;DTXSID30562262

Chemical Property of 4,4',4''-Methanetriyltris(N,N,3-trimethylaniline)

Chemical Property:

• XLogP3: 6.8
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 3
• Rotatable Bond Count: 6
• Exact Mass: 415.298748193
• Heavy Atom Count: 31
• Complexity: 468

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CC1=C(C=CC(=C1)N(C)C)C(C2=C(C=C(C=C2)N(C)C)C)C3=C(C=C(C=C3)N(C)C)C

Technology Process of 4,4',4''-Methanetriyltris(N,N,3-trimethylaniline)

There total 6 articles about 4,4',4''-Methanetriyltris(N,N,3-trimethylaniline) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 18.5%

N,N-dimethyl-m-toluidine (121-72-2) + sodium ethanolate (141-52-6) → bis(2-methyl-4-dimethylaminophenyl)-methane (71050-29-8) + tris(2-methyl-4-dimethylaminophenyl)methane (24619-07-6) + diethyl-N-methyl-N-(m-tolyl)-phosphoramidate + bis(2-methyl-4-dimethylaminophenyl)-ethylphosphinate

Guidance literature:

With trichlorophosphate; at 130 ℃; for 9h;

Reference yield: 6.5%

N,N-dimethyl-m-toluidine (121-72-2) → bis(2-methyl-4-dimethylaminophenyl)-methane (71050-29-8) + tris(2-methyl-4-dimethylaminophenyl)methane (24619-07-6) + diethyl-N-methyl-N-(m-tolyl)-phosphoramidate + bis(2-methyl-4-dimethylaminophenyl)-ethylphosphinate

Guidance literature:

With sodium ethanolate; trichlorophosphate; at 130 ℃; for 9h;

Reference yield:

N,N-dimethyl-m-toluidine (121-72-2) + 4,4'-Bis-dimethylamino-2,2'-dimethyl-benzhydrol (43001-46-3) → tris(2-methyl-4-dimethylaminophenyl)methane (24619-07-6)

Guidance literature:

With sulfuric acid;

upstream raw materials:

N,N-dimethyl-m-toluidine

4,4'-Bis-dimethylamino-2,2'-dimethyl-benzhydrol

orthoformic acid triethyl ester

sodium ethanolate

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