3-(3-Chlorophenyl)prop-2-enamide

Base Information

Chemical Name:3-(3-Chlorophenyl)prop-2-enamide
CAS No.:24654-56-6
Molecular Formula:C9H8ClNO
Molecular Weight:181.622
Hs Code.:2924299090
DSSTox Substance ID:DTXSID70702044
Mol file:24654-56-6.mol

Synonyms:24654-56-6;m-Chlorocinnamamide;3-(3-Chlorophenyl)prop-2-enamide;SCHEMBL2358452;3-(3-chloro-phenyl)-acrylamide;DTXSID70702044;PVASZFUVJJNHIM-UHFFFAOYSA-N;3-(3-CHLOROPHENYL)ACRYLAMIDE

Suppliers and Price of 3-(3-Chlorophenyl)prop-2-enamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 3 raw suppliers

Chemical Property of 3-(3-Chlorophenyl)prop-2-enamide

Chemical Property:

PSA：44.08000
LogP:2.98820
XLogP3:1.6
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:2
Exact Mass:181.0294416
Heavy Atom Count:12
Complexity:191

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC(=CC(=C1)Cl)C=CC(=O)N

Technology Process of 3-(3-Chlorophenyl)prop-2-enamide

There total 13 articles about 3-(3-Chlorophenyl)prop-2-enamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 3-chlorocinnamaldehyde oxime

: 24654-56-6,51791-24-3
3-(3-chloro-phenyl)-acrylamide

Guidance literature:: With [(eta.⁽⁵⁾-pentamethylcyclopentadienyl)Ir(H₂O)3](OTf)2; In water; at 120 ℃; for 12h; Schlenk technique;
DOI:10.1039/c3cy00934c

Reference yield: 75.0%

: 770-23-0,56578-37-1
(E)-3-(3-chlorophenyl)propenal

: 24654-56-6,51791-24-3
3-(3-chloro-phenyl)-acrylamide

Guidance literature:: (E)-3-(3-chlorophenyl)propenal; With hydroxylamine hydrochloride; sodium carbonate; In water; at 20 ℃; for 0.5h; Schlenk technique;

With [(eta.⁽⁵⁾-pentamethylcyclopentadienyl)Ir(H₂O)3](OTf)2; In water; at 110 ℃; for 12h;

Reference yield: 74.0%

: 1597410-53-1
(E)-S-methyl 4-(3-chlorophenyl)-2-oxobut-3-enethioate

: 24654-56-6,51791-24-3
3-(3-chloro-phenyl)-acrylamide

Guidance literature:: With diphenylphosphoranyl azide; copper(II) bis(trifluoromethanesulfonate); In water; N,N-dimethyl-formamide; at 100 ℃; for 3h;
DOI:10.1021/acs.joc.7b03054