2-(2-pyrrolidinylidene)-Acetic acid ethyl ester

Base Information

Chemical Name:2-(2-pyrrolidinylidene)-Acetic acid ethyl ester
CAS No.:25219-53-8
Molecular Formula:C₈H₁₃NO₂
Molecular Weight:155.197
Hs Code.:
Mol file:25219-53-8.mol

Synonyms:ethyl pyrrolidin-2-ylideneacetate;Acetic acid,2-pyrrolidinylidene-,ethyl ester;(Z)-ethyl 2-(pyrrolidin-2-ylidene)acetate;pyrrolidin-2-ylidene-acetic acid ethyl ester;2-Pyrrolidyliden-essigsaeure-ethylester;ethyl 2-pyrrolidylideneacetate;ethyl 2-(pyrrolidin-2-ylidene)acetate;ethyl pyrrolidinylidene acetate;

Suppliers and Price of 2-(2-pyrrolidinylidene)-Acetic acid ethyl ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 6 raw suppliers

Chemical Property of 2-(2-pyrrolidinylidene)-Acetic acid ethyl ester

Chemical Property:

PSA：38.33000
LogP:1.14560

Purity/Quality:: 97% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 2-(2-pyrrolidinylidene)-Acetic acid ethyl ester

There total 4 articles about 2-(2-pyrrolidinylidene)-Acetic acid ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 628-20-6
4-Chlorobutyronitrile

: 105-36-2
ethyl bromoacetate

: 25219-53-8,35150-22-2,108139-96-4
pyrrolidin-2-ylideneacetic acid ethyl ester

Guidance literature:: 4-Chlorobutyronitrile; ethyl bromoacetate; With methanesulfonic acid; zinc; In tetrahydrofuran; Inert atmosphere; Reflux;

With lithium hexamethyldisilazane; In tetrahydrofuran; at 0 - 20 ℃; for 5h; Inert atmosphere;
DOI:10.1055/s-0031-1290814

Reference yield: 29.0%

: 628-20-6
4-Chlorobutyronitrile

: 105-36-2
ethyl bromoacetate

: 7149-18-0
ethyl 2-amino-1-cyclopentene-1-carboxylate

: 25219-53-8,35150-22-2,108139-96-4
pyrrolidin-2-ylideneacetic acid ethyl ester

Guidance literature:: With methanesulfonic acid; zinc; In tetrahydrofuran; for 15h; chemoselective reaction; Reflux; Inert atmosphere;
DOI:10.1021/jo201964a