2,5-Dimethoxybenzene-1,3-dicarbaldehyde

Base Information

• Chemical Name: 2,5-Dimethoxybenzene-1,3-dicarbaldehyde
• CAS No.: 25224-72-0
• Molecular Formula: C10H10O4
• Molecular Weight: 194.187
• DSSTox Substance ID: DTXSID50541498
• Nikkaji Number: J1.056.066G
• Wikidata: Q82417869
• Mol file: 25224-72-0.mol

Synonyms:25224-72-0;2,5-dimethoxyisophthalaldehyde;2,5-Dimethoxybenzene-1,3-dicarbaldehyde;2,5-dimethoxy-benzene-1,3-dicarbaldehyde;SCHEMBL10728453;DTXSID50541498

Chemical Property of 2,5-Dimethoxybenzene-1,3-dicarbaldehyde

Chemical Property:

• XLogP3: 0.8
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 4
• Rotatable Bond Count: 4
• Exact Mass: 194.05790880
• Heavy Atom Count: 14
• Complexity: 186

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

• Canonical SMILES: COC1=CC(=C(C(=C1)C=O)OC)C=O

Technology Process of 2,5-Dimethoxybenzene-1,3-dicarbaldehyde

There total 8 articles about 2,5-Dimethoxybenzene-1,3-dicarbaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

[3-(hydroxymethyl)-2,5-dimethoxyphenyl]methanol (78840-04-7) → 1,4-dimethoxybenzene-2,6-dicarboxaldehyde (25224-72-0)

Guidance literature:

With barium permanganate; In dichloromethane; for 8h; Ambient temperature;

DOI:10.1016/S0040-4020(99)00055-1

Reference yield: 62.0%

[3-(hydroxymethyl)-2,5-dimethoxyphenyl]methanol (78840-04-7) → 1,4-dimethoxybenzene-2,6-dicarboxaldehyde (25224-72-0) + 2,5-dimethoxy-3-(hydroxymethyl)benzaldehyde (87050-66-6) + 2,5-dimethoxy-3-(3-oxo-1-butenyl)benzaldehyde (87050-67-7)

Guidance literature:

With pyridinium chlorochromate; In acetone; for 2.5h; Ambient temperature;

DOI:10.1021/jm00366a004

Reference yield: 62.0%

[3-(hydroxymethyl)-2,5-dimethoxyphenyl]methanol (78840-04-7) + acetone (67-64-1) → 1,4-dimethoxybenzene-2,6-dicarboxaldehyde (25224-72-0) + 2,5-dimethoxy-3-(hydroxymethyl)benzaldehyde (87050-66-6) + 2,5-dimethoxy-3-(3-oxo-1-butenyl)benzaldehyde (87050-67-7)

Guidance literature:

With pyridinium chlorochromate; for 2.5h; Ambient temperature;

DOI:10.1021/jm00366a004

upstream raw materials:

[3-(hydroxymethyl)-2,5-dimethoxyphenyl]methanol

1,4-dimethoxycyclohexa-1,4-diene

N,N-dimethyl-formamide

acetone

Downstream raw materials:

2,6-bis-1,4-dimethoxybenzene

2-Cyano-3-[3-(2,2-dicyano-vinyl)-2,5-dimethoxy-phenyl]-acrylonitrile

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