4-Pyridinecarboxamide, N-(2-bromophenyl)-N-methyl-

Base Information

Chemical Name:4-Pyridinecarboxamide, N-(2-bromophenyl)-N-methyl-
CAS No.:252930-63-5
Molecular Formula:C13H11BrN2O
Molecular Weight:291.147
Hs Code.:
DSSTox Substance ID:DTXSID00444501
Nikkaji Number:J1.250.358J
Wikidata:Q82262650
Mol file:252930-63-5.mol

Synonyms:4-Pyridinecarboxamide, N-(2-bromophenyl)-N-methyl-;252930-63-5;N-(2-Bromophenyl)-N-methylpyridine-4-carboxamide;DTXSID00444501

Suppliers and Price of 4-Pyridinecarboxamide, N-(2-bromophenyl)-N-methyl-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4-Pyridinecarboxamide, N-(2-bromophenyl)-N-methyl-

Chemical Property:

XLogP3:2.6
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:2
Exact Mass:290.00548
Heavy Atom Count:17
Complexity:266

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CN(C1=CC=CC=C1Br)C(=O)C2=CC=NC=C2

Technology Process of 4-Pyridinecarboxamide, N-(2-bromophenyl)-N-methyl-

There total 3 articles about 4-Pyridinecarboxamide, N-(2-bromophenyl)-N-methyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: 252930-61-3
N-(2-bromophenyl)-4-pyridinecarboxamide

: 74-88-4
methyl iodide

: 252930-63-5
N-(2-bromophenyl)-N-methyl-4-pyridinecarboxamide

Guidance literature:: With potassium hydroxide; In acetone; for 0.0833333h; Heating;
DOI:10.1021/jo9909498

Reference yield:

: 55-22-1
pyridine-4-carboxylic acid

: 252930-63-5
N-(2-bromophenyl)-N-methyl-4-pyridinecarboxamide

Guidance literature:: Multi-step reaction with 3 steps

1: thionyl chloride / 2 h / Heating

2: Py / 0 - 20 °C

3: 73 percent / KOH / acetone / 0.08 h / Heating

With pyridine; potassium hydroxide; thionyl chloride; In acetone; 1: Substitution / 2: Acylation / 3: Methylation;
DOI:10.1021/jo9909498

Reference yield:

: 14254-57-0
4-(chlorocarbonyl)pyridine

: 252930-63-5
N-(2-bromophenyl)-N-methyl-4-pyridinecarboxamide

Guidance literature:: Multi-step reaction with 2 steps

1: Py / 0 - 20 °C

2: 73 percent / KOH / acetone / 0.08 h / Heating

With pyridine; potassium hydroxide; In acetone; 1: Acylation / 2: Methylation;
DOI:10.1021/jo9909498