(N,N-diisopropyldithiocarbamato-S,S')bis(triphenylphosphine-P)gold(I) butane solvate

Base Information

Chemical Name:(N,N-diisopropyldithiocarbamato-S,S')bis(triphenylphosphine-P)gold(I) butane solvate
CAS No.:292840-58-5
Molecular Formula:C₄H₁₀*C₄₃H₄₄AuNP₂S₂
Molecular Weight:955.998
Hs Code.:

Synonyms:

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Chemical Property of (N,N-diisopropyldithiocarbamato-S,S')bis(triphenylphosphine-P)gold(I) butane solvate

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Technology Process of (N,N-diisopropyldithiocarbamato-S,S')bis(triphenylphosphine-P)gold(I) butane solvate

There total 1 articles about (N,N-diisopropyldithiocarbamato-S,S')bis(triphenylphosphine-P)gold(I) butane solvate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 4092-82-4
sodium N,N'-diisopropyldithiocarbamate

: 13453-07-1
gold(III) chloride

: 603-35-0
triphenylphosphine

: 106-97-8,9003-29-6,9021-92-5
n-butane

: 292840-58-5
(N,N-diisopropyldithiocarbamato-S,S')bis(triphenylphosphine-P)gold(I) butane solvate

Guidance literature:: In water; addn. of aq. soln. of Na compound to AuCl3 at room temp. under stirring;filtration; filtrate washed with H2O, dried overnight in vac.; solid di ssolved in butane and Ph3P was added at 353-363 K with stirring; soln. was refluxed for 4-5 h before cooling; slow evapn. at room temp. over a period of two weeks;
DOI:10.1107/S0108270100007319