2,5-Pyrrolidinedione, 1-[(4-methoxyphenyl)methyl]-3-(phenylmethoxy)-, (3S)-

Base Information

Chemical Name:2,5-Pyrrolidinedione, 1-[(4-methoxyphenyl)methyl]-3-(phenylmethoxy)-, (3S)-
CAS No.:254730-07-9
Molecular Formula:C19H19NO4
Molecular Weight:325.364
Hs Code.:
Mol file:254730-07-9.mol

Synonyms:(S)-3-Benzyloxy-1-(4-methoxy-benzyl)-pyrrolidine-2,5-dione;(S)-O-benzyl-1-(p-methoxybenzyl)malimide;

Suppliers and Price of 2,5-Pyrrolidinedione, 1-[(4-methoxyphenyl)methyl]-3-(phenylmethoxy)-, (3S)-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2,5-Pyrrolidinedione, 1-[(4-methoxyphenyl)methyl]-3-(phenylmethoxy)-, (3S)-

Chemical Property:

PSA：55.84000
LogP:2.47740

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 2,5-Pyrrolidinedione, 1-[(4-methoxyphenyl)methyl]-3-(phenylmethoxy)-, (3S)-

There total 3 articles about 2,5-Pyrrolidinedione, 1-[(4-methoxyphenyl)methyl]-3-(phenylmethoxy)-, (3S)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 100-39-0
benzyl bromide

: 254730-06-8
(S)-4-hydroxy-1-(4-methoxybenzyl)-2,5-pyrrolidinedione

: 254730-07-9
(S)-4-benzyloxy-1-(4-methoxybenzyl)-2,5-pyrrolidinedione

Guidance literature:: With silver(l) oxide; In diethyl ether; at 20 ℃; for 48h;
DOI:10.1016/S0957-4166(99)00395-X

Reference yield:

: 174874-82-9
acetic acid (3S)-1-(4-methoxy-benzyl)-2,5-dioxo-pyrrolidin-3-yl ester

: 254730-07-9
(S)-4-benzyloxy-1-(4-methoxybenzyl)-2,5-pyrrolidinedione

Guidance literature:: Multi-step reaction with 2 steps

1: 91 percent / AcCl; EtOH / 5 h / 50 °C

2: 94 percent / Ag₂O / diethyl ether / 48 h / 20 °C

With ethanol; acetyl chloride; silver(l) oxide; In diethyl ether; 1: Deacetylation / 2: Substitution;
DOI:10.1016/S0957-4166(99)00395-X

Reference yield:

: 2393-23-9
4-methoxy-benzylamine

: 254730-07-9
(S)-4-benzyloxy-1-(4-methoxybenzyl)-2,5-pyrrolidinedione

Guidance literature:: Multi-step reaction with 2 steps

1: 5,5-dimethyl-1,3-cyclohexadiene; water / 8 h / Reflux

2: silver(l) oxide / tetrahydrofuran / 20 °C

With silver(l) oxide; In tetrahydrofuran; 5,5-dimethyl-1,3-cyclohexadiene; water;