{4-[(4-chlorophenyl)sulfanyl]phenyl}hydrazine

Base Information

• Chemical Name: {4-[(4-chlorophenyl)sulfanyl]phenyl}hydrazine
• CAS No.: 75787-58-5
• Molecular Formula: C12H11ClN2S
• Molecular Weight: 250.752

Synonyms:Hydrazine,[p-(p-chlorophenylthio)phenyl]- (6CI);{4-[(4-chlorophenyl)sulfanyl]phenyl}hydrazine;[4-(4-chlorophenyl)sulfanylphenyl]hydrazine;Hydrazine, (4-((4-chlorophenyl)thio)phenyl)-;

Chemical Property of {4-[(4-chlorophenyl)sulfanyl]phenyl}hydrazine

Chemical Property:

• Vapor Pressure: 2.66E-08mmHg at 25°C
• Refractive Index: 1.692
• Boiling Point: 450.3 °C at 760 mmHg
• Flash Point: 226.2 °C
• Density: 1.34 g/cm³

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of {4-[(4-chlorophenyl)sulfanyl]phenyl}hydrazine

There total 2 articles about {4-[(4-chlorophenyl)sulfanyl]phenyl}hydrazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 52.0%

p-Chlorothiophenol (106-54-7) + phenylhydrazine (100-63-0) → (4-(4-chlorophenylthio)phenyl)hydrazine (75787-58-5)

Guidance literature:

With di-tert-butyl peroxide; iodine; at 120 ℃; for 24h; Inert atmosphere; Sealed tube;

DOI:10.1021/acs.joc.5b00540

Reference yield:

→ (4-(4-chlorophenylthio)phenyl)hydrazine (75787-58-5)

Guidance literature:

With hydrogenchloride; tin(ll) chloride;

DOI:10.1021/ja01548a032

Reference yield:

ethyl 3-(2-furyl)-3-oxopropanoate (615-09-8) + (4-(4-chlorophenylthio)phenyl)hydrazine (75787-58-5) → 2-[4-(4-chloro-phenylsulfanyl)-phenyl]-5-[2]furyl-1,2-dihydro-pyrazol-3-one

Guidance literature:

upstream raw materials:

p-Chlorothiophenol

phenylhydrazine

Downstream raw materials:

1-[4-(4-chloro-phenylsulfanyl)-phenyl]-5-dimethylcarbamoyloxy-3-methyl-1H-pyrazole

1-[4-(4-chloro-phenylsulfanyl)-phenyl]-5-dimethylcarbamoyloxy-3-phenyl-1H-pyrazole

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