Diethyl 4-acetylphenylphosphonate

Base Information

Chemical Name:Diethyl 4-acetylphenylphosphonate
CAS No.:25944-71-2
Molecular Formula:C12H17O4P
Molecular Weight:256.238
Hs Code.:2931900090
DSSTox Substance ID:DTXSID70464458
Nikkaji Number:J505.461C
Wikidata:Q82289778
Mol file:25944-71-2.mol

Synonyms:Diethyl 4-acetylphenylphosphonate;25944-71-2;(4-ACETYL-PHENYL)-PHOSPHONIC ACID DIETHYL ESTER;(4-Acetyl-phenyl)phosphonic acid diethyl ester;DTXSID70464458;diethyl 4-acetyl-phenylphosphonate;diethyl (4-acetylphenyl)phosphonate;AKOS015962588;FT-0738077;J-520296

Suppliers and Price of Diethyl 4-acetylphenylphosphonate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

American Custom Chemicals Corporation
DIETHYL 4-ACETYLPHENYLPHOSPHONATE 95.00%
100MG
$ 525.00

Total 4 raw suppliers

Chemical Property of Diethyl 4-acetylphenylphosphonate

Chemical Property:

Vapor Pressure:2.67E-05mmHg at 25°C
Boiling Point:357.7oC at 760 mmHg
Flash Point:183.8oC
PSA：62.41000
Density:1.14g/cm3
LogP:2.78060
XLogP3:1.4
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:6
Exact Mass:256.08644602
Heavy Atom Count:17
Complexity:285

Purity/Quality:

85.0-99.8% ^*data from raw suppliers

DIETHYL 4-ACETYLPHENYLPHOSPHONATE 95.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CCOP(=O)(C1=CC=C(C=C1)C(=O)C)OCC

Technology Process of Diethyl 4-acetylphenylphosphonate

There total 27 articles about Diethyl 4-acetylphenylphosphonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 13329-40-3
4-Iodoacetophenone

: 122-52-1
triethyl phosphite

: 25944-71-2
diethyl (4-acetylphenyl)phosphonate

Guidance literature:: With tributyl-amine; (4s,6s)-2,4,5,6-tetra(9H-carbazol-9-yl)isophthalonitrile; N,N,N',N'-tetramethylguanidine; In water; dimethyl sulfoxide; at 20 ℃; for 16h; Irradiation;
DOI:10.1039/d0sc04387g

Reference yield: 93.0%

: 1-(4-acetylbenzoyl)piperidine-2,6-dione

: 762-04-9
phosphonic acid diethyl ester

: 25944-71-2
diethyl (4-acetylphenyl)phosphonate

Guidance literature:: With palladium diacetate; triethylamine; 1,4-di(diphenylphosphino)-butane; In 1,4-dioxane; at 160 ℃; for 15h; Reagent/catalyst; Inert atmosphere; Schlenk technique;
DOI:10.1002/anie.201707102