1-(4-Methoxybenzyl)-2-(4-methoxyphenyl)-1H-benzo[d]imidazole

Base Information

• Chemical Name: 1-(4-Methoxybenzyl)-2-(4-methoxyphenyl)-1H-benzo[d]imidazole
• CAS No.: 2620-83-9
• Molecular Formula: C22H20N2O2
• Molecular Weight: 344.413
• Hs Code.: 2933990090
• DSSTox Substance ID: DTXSID10353599
• Nikkaji Number: J2.293.775H
• Wikidata: Q82131281
• ChEMBL ID: CHEMBL1531383
• Mol file: 2620-83-9.mol

Synonyms:1-(4-methoxybenzyl)-2-(4-methoxyphenyl)-1H-benzo(d)imidazole;MBMPB

Chemical Property of 1-(4-Methoxybenzyl)-2-(4-methoxyphenyl)-1H-benzo[d]imidazole

Chemical Property:

• PSA: 36.28000
• LogP: 4.76880
• Storage Temp.: 2-8°C
• XLogP3: 4.6
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 3
• Rotatable Bond Count: 5
• Exact Mass: 344.152477885
• Heavy Atom Count: 26
• Complexity: 430

Purity/Quality:

97% ^*data from raw suppliers

1-(4-methoxybenzyl)-2-(4-methoxyphenyl)-1H-benzo[d]imidazole 95% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: COC1=CC=C(C=C1)CN2C3=CC=CC=C3N=C2C4=CC=C(C=C4)OC

Technology Process of 1-(4-Methoxybenzyl)-2-(4-methoxyphenyl)-1H-benzo[d]imidazole

There total 23 articles about 1-(4-Methoxybenzyl)-2-(4-methoxyphenyl)-1H-benzo[d]imidazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

4-methoxy-benzaldehyde (123-11-5) + 1,2-diamino-benzene (95-54-5) → 1-(4-methoxybenzyl)-2-(4-methoxyphenyl)-1H-benzimidazole (2620-83-9)

Guidance literature:

With ytterbium(III) chloride; for 8h; Sonication; neat (no solvent);

DOI:10.1080/00397911.2010.524337

Reference yield: 98.0%

4-methoxy-benzaldehyde (123-11-5) + 1,2-diamino-benzene (95-54-5) → 2-(4-methoxyphenyl)-1H-benzimidazole (2620-81-7) + 1-(4-methoxybenzyl)-2-(4-methoxyphenyl)-1H-benzimidazole (2620-83-9)

Guidance literature:

With silica gel supported trichloroacetic acid; In ethanol; water; at 50 ℃; for 0.133333h; regioselective reaction; Sonication; Green chemistry;

DOI:10.1007/s12039-014-0662-4

Reference yield: 94.0%

N,N'-bis-(4-methoxy-benzylidene)-benzene-1,2-diamine (74661-51-1) → 1-(4-methoxybenzyl)-2-(4-methoxyphenyl)-1H-benzimidazole (2620-83-9)

Guidance literature:

With toluene-4-sulfonic acid; In neat (no solvent); Milling; Green chemistry;

DOI:10.1134/S1070428020090201

upstream raw materials:

o-phenylenediamine hydrochloride

4-methoxy-benzaldehyde

2-(p-methoxyphenyl)-4,4-dimethyloxazolidine

1,2-diamino-benzene

Downstream raw materials:

Cd(1-(p-methoxybenzyl)-2-(p-methoxyphenyl)benzimidazole)2Cl₂

Zn(1-(p-methoxybenzyl)-2-(p-methoxyphenyl)benzimidazole)2Br₂

Hg(1-(p-methoxybenzyl)-2-(p-methoxyphenyl)benzimidazole)2Br₂

Zn(1-(p-methoxybenzyl)-2-(p-methoxyphenyl)benzimidazole)2Cl₂

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