(Z)-1,2-Diacetoxy-1,2-diphenylethene

Base Information

• Chemical Name: (Z)-1,2-Diacetoxy-1,2-diphenylethene
• CAS No.: 26431-43-6
• Molecular Formula: C18H16O4
• Molecular Weight: 296.323
• Hs Code.: 2915390090
• Mol file: 26431-43-6.mol

Synonyms:1,2-Ethenediol,1,2-diphenyl-,diacetate,(E);1,2-Ethenediol,1,2-diphenyl-,diacetate,(1Z);

Chemical Property of (Z)-1,2-Diacetoxy-1,2-diphenylethene

Chemical Property:

• PSA: 115.06000
• LogP: 3.81020

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of (Z)-1,2-Diacetoxy-1,2-diphenylethene

There total 15 articles about (Z)-1,2-Diacetoxy-1,2-diphenylethene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

1,2-Bis-(trimethylsilyloxy)-1,2-diphenylethylen (37980-77-1) + acetic anhydride (108-24-7) → (Z)-1,2-diphenylethene-1,2-diyl diacetate (26431-43-6)

Guidance literature:

With 4-pyrrolidin-1-ylpyridine; triethylamine; for 7h; Ambient temperature;

Reference yield: 84.0%

acetic anhydride (108-24-7) + benzil (134-81-6) → (Z)-1,2-diphenylethene-1,2-diyl diacetate (26431-43-6)

Guidance literature:

With lithium perchlorate; In acetone; at 15 ℃; electrolysis, -0.9 V vs SCE, 2 F/mol;

Reference yield:

tetrahydrofuran (109-99-9,24979-97-3,77392-70-2) + acetyl chloride (75-36-5) → 4-Chlorobutyl acetate (6962-92-1) + (Z)-1,2-diphenylethene-1,2-diyl diacetate (26431-43-6) + (E)-O,O'-diacetyl-1,2-diphenylethen-1,2-diol (35855-69-7)

Guidance literature:

With lithium amalgam; benzoyl chloride;

upstream raw materials:

acetic anhydride

Desyl chloride

benzil

sodium acetate

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