1-N,2-N-bis(4-bromophenyl)acenaphthylene-1,2-diimine

Base Information

Chemical Name:1-N,2-N-bis(4-bromophenyl)acenaphthylene-1,2-diimine
CAS No.:266340-77-6
Molecular Formula:C₂₄H₁₄Br₂N₂
Molecular Weight:490.197
Hs Code.:
DSSTox Substance ID:DTXSID20365305
Nikkaji Number:J1.939.910I
Mol file:266340-77-6.mol

Synonyms:1-N,2-N-bis(4-bromophenyl)acenaphthylene-1,2-diimine;266340-77-6;N-(4-bromophenyl)-N-(2-[(4-bromophenyl)imino]-1(2H)-acenaphthylenylidene)amine;AP-835/40885068;DTXSID20365305;bis(4-bromophenylimino)acenaphthene;N,N'-Bis(4-bromophenyl)-1,2-acenaphthenediimine;N,N/'-Bis(4-bromophenyl)-1,2-acenaphthenediimine

Suppliers and Price of 1-N,2-N-bis(4-bromophenyl)acenaphthylene-1,2-diimine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-N,2-N-bis(4-bromophenyl)acenaphthylene-1,2-diimine

Chemical Property:

PSA：24.72000
LogP:7.62000
XLogP3:7.3
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:2
Exact Mass:489.95032
Heavy Atom Count:28
Complexity:562

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC2=C3C(=C1)C(=NC4=CC=C(C=C4)Br)C(=NC5=CC=C(C=C5)Br)C3=CC=C2

Technology Process of 1-N,2-N-bis(4-bromophenyl)acenaphthylene-1,2-diimine

There total 1 articles about 1-N,2-N-bis(4-bromophenyl)acenaphthylene-1,2-diimine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

: 106-40-1
4-bromo-aniline

: 82-86-0
acenaphthene quinone

: 266340-77-6
(C₆H₄Br)2N₂C₂C₁₀H₆

Guidance literature:: With trifluoroacetic anhydride; for 3h; Milling;
DOI:10.1039/c6dt00978f

Reference yield: 84.0%

: indium(III) chloride

: 266340-77-6
(C₆H₄Br)2N₂C₂C₁₀H₆

: 7732-18-5
water

: C₂₄H₁₆Br₂Cl₃InN₂O

Guidance literature:: for 2h; Solvent; Milling;
DOI:10.1039/c6dt00978f

Reference yield: 28.0%

: 14099-01-5
rhenium(I) pentacarbonyl chloride

: 266340-77-6
(C₆H₄Br)2N₂C₂C₁₀H₆

: 266340-75-4
Re(CO)3Cl(C₆H₄Br)2N₂C₂C₁₀H₆

Guidance literature:: In toluene; suspn. of Re-complex and ligand in toluene was refluxed for 30 min, cooled to room temp.; pptn. by addn. of n-hexane, purified by chromy. on silica gel with CH2Cl2 as eluent; elem. anal.;