3-(BENZYLOXY)-4-ETHOXYBENZALDEHYDE

Base Information

• Chemical Name: 3-(BENZYLOXY)-4-ETHOXYBENZALDEHYDE
• CAS No.: 26691-25-8
• Molecular Formula: C16H16O3
• Molecular Weight: 256.301
• Mol file: 26691-25-8.mol

Synonyms:3-benzyloxy-4-ethoxy-benzaldehyde;3-benzyloxy-4-ethoxybenzaldehyde;3-Benzyloxy-4-ethoxybenzaldehyd;4-ethoxy-3-benzyloxybenzaldehyde;

Chemical Property of 3-(BENZYLOXY)-4-ETHOXYBENZALDEHYDE

Chemical Property:

• Melting Point: 69.8 - 70.8 °C
• PSA: 35.53000
• LogP: 3.47680

Purity/Quality:

99% ^*data from raw suppliers

3-(Benzyloxy)-4-ethoxybenzaldehyde 95% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 3-(BENZYLOXY)-4-ETHOXYBENZALDEHYDE

There total 9 articles about 3-(BENZYLOXY)-4-ETHOXYBENZALDEHYDE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

4-ethoxy-3-hydroxybenzaldehyde (2539-53-9) + benzyl chloride (100-44-7) → 3-(benzyloxy)-4-ethoxybenzaldehyde (26691-25-8)

Guidance literature:

With potassium carbonate; In ethanol; at 90 ℃; for 2.5h; Inert atmosphere;

Reference yield:

ethyl bromide (74-96-4) + 3-benzyloxy-4-hydroxybenzaldehyde (50773-56-3) → 3-(benzyloxy)-4-ethoxybenzaldehyde (26691-25-8)

Guidance literature:

3-benzyloxy-4-hydroxybenzaldehyde; With potassium carbonate; In N,N-dimethyl-formamide; at 40 ℃; for 0.166667h;

ethyl bromide; In N,N-dimethyl-formamide; at 70 ℃;

DOI:10.1016/j.cclet.2015.05.003

Reference yield:

4-ethoxy-3-hydroxybenzaldehyde (2539-53-9) + potassium carbonate (584-08-7) + benzyl chloride (100-44-7) → 3-(benzyloxy)-4-ethoxybenzaldehyde (26691-25-8)

Guidance literature:

In N,N-dimethyl-formamide;

upstream raw materials:

4-ethoxy-3-hydroxybenzaldehyde

benzyl chloride

3,4-dihydroxybenzaldehyde

potassium carbonate

Downstream raw materials:

4-Ethoxy-3-hydroxyphenylessigsaeure

methyl (4-ethoxy-3-hydroxyphenyl)acetate

methyl (3-benzyloxy-4-ethoxyphenyl)acetate

6'-Ethoxy-4,5-dimethoxy-2,3'-bis(methoxycarbonylmethyl)phenoxybenzol