Ethanedial bis(dimethylhydrazone)

Base Information

• Chemical Name: Ethanedial bis(dimethylhydrazone)
• CAS No.: 26757-28-8
• Molecular Formula: C6H14N4
• Molecular Weight: 142.204
• DSSTox Substance ID: DTXSID101265597
• Mol file: 26757-28-8.mol

Synonyms:ethanedial bis(dimethylhydrazone);SCHEMBL14799498;DTXSID101265597;glyoxal bis(N,N-dimethylhydrazone);26757-28-8;Ethanedial, 1,2-bis(2,2-dimethylhydrazone)

Chemical Property of Ethanedial bis(dimethylhydrazone)

Chemical Property:

• Boiling Point: 103 °C (6 mmHg)
• PSA: 31.20000
• LogP: 0.08120
• XLogP3: 1.1
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 4
• Rotatable Bond Count: 3
• Exact Mass: 142.121846464
• Heavy Atom Count: 10
• Complexity: 110

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CN(C)N=CC=NN(C)C

Technology Process of Ethanedial bis(dimethylhydrazone)

There total 1 articles about Ethanedial bis(dimethylhydrazone) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

N,N-Dimethylhydrazine (57-14-7) + acetone (67-64-1) → 1,3-dimethyl-1H-pyrazole (694-48-4) + tetramethylhydrazine (6415-12-9) + Acetone dimethylhydrazone (13483-31-3) + N-Nitrosodimethylamine (62-75-9) + acetaldehydedimethylhydrazone (7422-90-4) + 1,2-bis(2-methyl-2-phenylhydrazone) (26757-28-8) + propan-2-one azine (627-70-3)

Guidance literature:

With shungite;

DOI:10.1134/S1070363214060097

Reference yield: 68.0%

1,2-bis(2-methyl-2-phenylhydrazone) (26757-28-8) + p-nitrobenzonitrile oxide (2574-03-0) → 4-dimethylamino-5-(dimethylhydrazonomethyl)-3-(4-nitrophenyl)-Δ2-1,2,4-oxadiazoline (134918-38-0)

Guidance literature:

In acetonitrile;

DOI:10.1007/BF00476760

Reference yield:

1,2-bis(2-methyl-2-phenylhydrazone) (26757-28-8) → glyoxime (557-30-2)

Guidance literature:

With hydroxylamine hydrochloride;

upstream raw materials:

N,N-Dimethylhydrazine

acetone

Downstream raw materials:

glyoxime

4-dimethylamino-5-(dimethylhydrazonomethyl)-3-(4-nitrophenyl)-Δ²-1,2,4-oxadiazoline

Refernces