5H-Dibenzo[a,i]carbazole, 6,13-dihydro-

Base Information

Chemical Name:5H-Dibenzo[a,i]carbazole, 6,13-dihydro-
CAS No.:63039-79-2
Molecular Formula:C20H15 N
Molecular Weight:269.346
Hs Code.:
NSC Number:109910
DSSTox Substance ID:DTXSID40296561
Wikidata:Q82037215

Synonyms:5H-Dibenzo[a,i]carbazole, 6,13-dihydro-;63039-79-2;NSC109910;DTXSID40296561;5H-Dibenzo[a, 6,13-dihydro-;NSC-109910

Suppliers and Price of 5H-Dibenzo[a,i]carbazole, 6,13-dihydro-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 5 raw suppliers

Chemical Property of 5H-Dibenzo[a,i]carbazole, 6,13-dihydro-

Chemical Property:

Vapor Pressure:3.71E-10mmHg at 25°C
Boiling Point:513.8°C at 760 mmHg
Flash Point:231.1°C
Density:1.266g/cm³
XLogP3:5.3
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:0
Rotatable Bond Count:0
Exact Mass:269.120449483
Heavy Atom Count:21
Complexity:391

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1CC2=C(C3=CC=CC=C31)NC4=C2C=CC5=CC=CC=C54

Technology Process of 5H-Dibenzo[a,i]carbazole, 6,13-dihydro-

There total 1 articles about 5H-Dibenzo[a,i]carbazole, 6,13-dihydro- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 2243-56-3
1-naphthylhydrazine hydrochloride

: 529-34-0
3,4-dihydronaphthalene-1(2H)-one

: 63039-79-2
6,13-dihydro-5H-dibenzo[a,i]carbazole

Guidance literature:: With acetic acid; In ethanol; for 3h;

Reference yield: 90.0%

: 63039-79-2
6,13-dihydro-5H-dibenzo[a,i]carbazole

: 239-64-5
13H-dibenzocarbazole

Guidance literature:: With 2,3-dicyano-5,6-dichloro-p-benzoquinone; In acetonitrile; at 20 ℃; for 3h;

Reference yield:

: 63039-79-2
6,13-dihydro-5H-dibenzo[a,i]carbazole

: C₄₄H₃₀NOP

Guidance literature:: Multi-step reaction with 2 steps

1: 2,3-dicyano-5,6-dichloro-p-benzoquinone / acetonitrile / 3 h / 20 °C

2: sodium t-butanolate; bis(tri-t-butylphosphine)palladium⁽⁰⁾ / toluene / 3 h

With bis(tri-t-butylphosphine)palladium⁽⁰⁾; 2,3-dicyano-5,6-dichloro-p-benzoquinone; sodium t-butanolate; In toluene; acetonitrile;