Succinic acid 3-{3-[2-(2-benzoyloxy-ethoxy)-ethoxycarbonyl]-propionyloxy}-2-bromo-2-nitro-propyl ester 2-(2-benzoyloxy-ethoxy)-ethyl ester

Base Information

• Chemical Name: Succinic acid 3-{3-[2-(2-benzoyloxy-ethoxy)-ethoxycarbonyl]-propionyloxy}-2-bromo-2-nitro-propyl ester 2-(2-benzoyloxy-ethoxy)-ethyl ester
• CAS No.: 125867-97-2
• Molecular Formula: C₃₃H₃₈BrNO₁₆
• Molecular Weight: 784.566
• Mol file: 125867-97-2.mol

Synonyms:

Chemical Property of Succinic acid 3-{3-[2-(2-benzoyloxy-ethoxy)-ethoxycarbonyl]-propionyloxy}-2-bromo-2-nitro-propyl ester 2-(2-benzoyloxy-ethoxy)-ethyl ester

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of Succinic acid 3-{3-[2-(2-benzoyloxy-ethoxy)-ethoxycarbonyl]-propionyloxy}-2-bromo-2-nitro-propyl ester 2-(2-benzoyloxy-ethoxy)-ethyl ester

There total 3 articles about Succinic acid 3-{3-[2-(2-benzoyloxy-ethoxy)-ethoxycarbonyl]-propionyloxy}-2-bromo-2-nitro-propyl ester 2-(2-benzoyloxy-ethoxy)-ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

diethylene glycol benzoate (20587-61-5) → Succinic acid 3-{3-[2-(2-benzoyloxy-ethoxy)-ethoxycarbonyl]-propionyloxy}-2-bromo-2-nitro-propyl ester 2-(2-benzoyloxy-ethoxy)-ethyl ester (125867-97-2)

Guidance literature:

Multi-step reaction with 2 steps

2: 1) pyridine, Cl-COOEt / 1) ether, -10 degC, 20 min.; 2) ether, 24 h, room temp.

With pyridine; chloroformic acid ethyl ester;

Reference yield:

benzoyl chloride (98-88-4) → Succinic acid 3-{3-[2-(2-benzoyloxy-ethoxy)-ethoxycarbonyl]-propionyloxy}-2-bromo-2-nitro-propyl ester 2-(2-benzoyloxy-ethoxy)-ethyl ester (125867-97-2)

Guidance literature:

Multi-step reaction with 3 steps

1: pyridine

3: 1) pyridine, Cl-COOEt / 1) ether, -10 degC, 20 min.; 2) ether, 24 h, room temp.

With pyridine; chloroformic acid ethyl ester;

Reference yield:

2-bromo-2-nitro-1,3-propanediol (52-51-7) + Succinic acid mono-[2-(2-benzoyloxy-ethoxy)-ethyl] ester (125867-95-0) → Succinic acid 2-(2-benzoyloxy-ethoxy)-ethyl ester 2-bromo-3-hydroxy-2-nitro-propyl ester (125867-96-1) + Succinic acid 3-{3-[2-(2-benzoyloxy-ethoxy)-ethoxycarbonyl]-propionyloxy}-2-bromo-2-nitro-propyl ester 2-(2-benzoyloxy-ethoxy)-ethyl ester (125867-97-2)

Guidance literature:

With pyridine; chloroformic acid ethyl ester; Yield given. Multistep reaction. Yields of byproduct given; 1) ether, -10 degC, 20 min.; 2) ether, 24 h, room temp.;

upstream raw materials:

2-bromo-2-nitro-1,3-propanediol

Succinic acid mono-[2-(2-benzoyloxy-ethoxy)-ethyl] ester

diethylene glycol benzoate

benzoyl chloride

Refernces