6-Iodo-2-hexyne

Base Information

• Chemical Name: 6-Iodo-2-hexyne
• CAS No.: 28077-74-9
• Molecular Formula: C6H9I
• Molecular Weight: 208.042
• Hs Code.: 2903399090
• Mol file: 28077-74-9.mol

Synonyms:6-Iodo-2-hexyne;2-Hexyne,6-iodo;

Chemical Property of 6-Iodo-2-hexyne

Chemical Property:

• PSA: 0.00000
• LogP: 2.22490

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 6-Iodo-2-hexyne

There total 10 articles about 6-Iodo-2-hexyne which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

1-chloro-4-pentyne (14267-92-6) + methyl iodide (74-88-4) → 6-iodo-2-hexyne (28077-74-9)

Guidance literature:

With n-butyllithium; sodium iodide; In tetrahydrofuran; [⁽²⁾H₆]acetone; water;

Reference yield: 82.0%

1-chloro-4-pentyne (14267-92-6) → 6-iodo-2-hexyne (28077-74-9)

Guidance literature:

1-chloro-4-pentyne; With n-butyllithium; In tetrahydrofuran; at -78 ℃; for 0.5h;

With methyl iodide; In tetrahydrofuran; for 2h; Reflux;

With sodium iodide; In tetrahydrofuran; acetone; for 22h; Reflux;

Reference yield: 67.0%

methanesulfonic acid hex-4-ynyl ester (68275-05-8) → 6-iodo-2-hexyne (28077-74-9)

Guidance literature:

With sodium iodide; In acetone; for 5h; Reflux;

upstream raw materials:

6-chlorohex-2-yne

1-chloro-4-pentyne

methyl iodide

pent-1-yn-5-ol

Downstream raw materials:

(1E)-1-phenylnon-1-en-7-yn-3-ol

(S)-2-(((9H-fluoren-9-yl)methoxy)carbonylamino)-2-methyloct-6-ynoic acid