2-METHOXY-4'-METHYLBENZOPHENONE

Base Information

• Chemical Name: 2-METHOXY-4'-METHYLBENZOPHENONE
• CAS No.: 28137-36-2
• Molecular Formula: C15H14O2
• Molecular Weight: 226.275
• Hs Code.: 2914509090
• Mol file: 28137-36-2.mol

Synonyms:(2-methoxyphenyl)(p-tolyl)methanone;(2-methoxyphenyl)(4-methylphenyl)methanone;2-METHOXY-4'-METHYLBENZOPHENONE;Benzophenone,2-methoxy-4'-methyl;

Chemical Property of 2-METHOXY-4'-METHYLBENZOPHENONE

Chemical Property:

• Vapor Pressure: 2.86E-06mmHg at 25°C
• Melting Point: 64–65°C
• Boiling Point: 389.4oC at 760 mmHg
• Flash Point: 179.4oC
• PSA: 26.30000
• Density: 1.088g/cm3
• LogP: 3.23460

Purity/Quality:

97% ^*data from raw suppliers

2-methoxy-4'-methylbenzophenone 97% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
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MSDS Files:

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Technology Process of 2-METHOXY-4'-METHYLBENZOPHENONE

There total 20 articles about 2-METHOXY-4'-METHYLBENZOPHENONE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

carbon monoxide (201230-82-2) + 4,4'-dimethyldiphenyliodonium fluoroborate + potassium (2-methoxyphenyl)trifluoroborate → (2-methoxyphenyl)(4-methylphenyl)methanone (28137-36-2)

Guidance literature:

With palladium diacetate; potassium carbonate; In 1,2-dimethoxyethane; at 20 ℃; for 2h; under 760 Torr;

DOI:10.1039/a900963i

Reference yield: 82.0%

(4-methylphenyl)(2'-methoxyphenyl)methanol → (2-methoxyphenyl)(4-methylphenyl)methanone (28137-36-2)

Guidance literature:

With cesium hydroxide; air; In toluene; at 110 ℃; for 24h;

DOI:10.1016/j.tetlet.2008.06.061

Reference yield: 77.0%

chloroform (67-66-3,8013-54-5) + 4-tolyl iodide (624-31-7) + potassium (2-methoxyphenyl)trifluoroborate → (2-methoxyphenyl)(4-methylphenyl)methanone (28137-36-2)

Guidance literature:

With cesiumhydroxide monohydrate; sodium carbonate; sodium iodide; iron(II) chloride; Trimethylacetic acid; at 120 ℃; for 28h; chemoselective reaction; Green chemistry;

DOI:10.1039/c6gc02158a

upstream raw materials:

4-methyl-benzoyl chloride

methoxybenzene

2,3,4,5,6-pentamethylphenyl 4-tolyl ketone

2-Methoxybenzoic acid

Downstream raw materials:

2-hydroxy-4'-methylbenzophenone

C₁₈H₂₀O₂

C₁₈H₁₈O₂

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