[(3,5-Dimethyl-1,2-oxazol-4-yl)methyl](triphenyl)phosphanium chloride

Base Information

Chemical Name:[(3,5-Dimethyl-1,2-oxazol-4-yl)methyl](triphenyl)phosphanium chloride
CAS No.:28241-32-9
Molecular Formula:C24H23NOP.Cl
Molecular Weight:407.879
Hs Code.:
DSSTox Substance ID:DTXSID90606070
Mol file:28241-32-9.mol

Synonyms:28241-32-9;SCHEMBL11629945;DTXSID90606070;KFOHZYYNAVQQQO-UHFFFAOYSA-M;[(3,5-Dimethyl-1,2-oxazol-4-yl)methyl](triphenyl)phosphanium chloride;(3,5-dimethyl-4-isoxazolylmethyl)triphenyl-phosphonium chloride;(3,5-dimethyl-4-isoxazolylmethyl)triphenylphosphonium chloride

Suppliers and Price of [(3,5-Dimethyl-1,2-oxazol-4-yl)methyl](triphenyl)phosphanium chloride

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of [(3,5-Dimethyl-1,2-oxazol-4-yl)methyl](triphenyl)phosphanium chloride

Chemical Property:

Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:5
Exact Mass:407.1205790
Heavy Atom Count:28
Complexity:406

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=C(C(=NO1)C)C[P+](C2=CC=CC=C2)(C3=CC=CC=C3)C4=CC=CC=C4.[Cl-]

Technology Process of [(3,5-Dimethyl-1,2-oxazol-4-yl)methyl](triphenyl)phosphanium chloride

There total 3 articles about [(3,5-Dimethyl-1,2-oxazol-4-yl)methyl](triphenyl)phosphanium chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 19788-37-5
4-chloromethyl-3,5-dimethylisoxazole

: 603-35-0
triphenylphosphine

: 28241-32-9
(3,5-dimethyl-isoxazol-4-ylmethyl)-triphenyl-phosphonium; chloride

Guidance literature:: In dichloromethane; for 6h; Reflux; Inert atmosphere;
DOI:10.1039/c3ra00029j

Reference yield:

: 300-87-8
3,5-dimethyl-1,2-oxazole

: 28241-32-9
(3,5-dimethyl-isoxazol-4-ylmethyl)-triphenyl-phosphonium; chloride

Guidance literature:: Multi-step reaction with 2 steps

1: 40 percent / HCl, ZnCl₂ / acetic acid / 3 h / 35 - 40 °C

2: 76 percent / xylene / 22.5 h / Heating

With hydrogenchloride; zinc(II) chloride; In acetic acid; xylene;
DOI:10.1055/s-1998-2126