[(CO)3(((C₆H₅)2PCH₂)2)Mn(CCC(CH₃)3)]Cu[P(C₆H₄CH₃)3]⁽¹⁺⁾*PF₆^(1-)=[((CO)3(((C₆H₅)2PCH₂)2)Mn(C₆H₉))Cu(PC₂₁H₂₁)]PF₆

Base Information

• Chemical Name: [(CO)3(((C₆H₅)2PCH₂)2)Mn(CCC(CH₃)3)]Cu[P(C₆H₄CH₃)3]⁽¹⁺⁾*PF₆^(1-)=[((CO)3(((C₆H₅)2PCH₂)2)Mn(C₆H₉))Cu(PC₂₁H₂₁)]PF₆
• CAS No.: 105560-20-1
• Molecular Formula: C₅₆H₅₄CuMnO₃P₃*F₆P
• Molecular Weight: 1131.41
• Mol file: 105560-20-1.mol

Synonyms:

Chemical Property of [(CO)3(((C₆H₅)2PCH₂)2)Mn(CCC(CH₃)3)]Cu[P(C₆H₄CH₃)3]⁽¹⁺⁾*PF₆^(1-)=[((CO)3(((C₆H₅)2PCH₂)2)Mn(C₆H₉))Cu(PC₂₁H₂₁)]PF₆

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of [(CO)3(((C₆H₅)2PCH₂)2)Mn(CCC(CH₃)3)]Cu[P(C₆H₄CH₃)3]⁽¹⁺⁾*PF₆^(1-)=[((CO)3(((C₆H₅)2PCH₂)2)Mn(C₆H₉))Cu(PC₂₁H₂₁)]PF₆

There total 2 articles about [(CO)3(((C₆H₅)2PCH₂)2)Mn(CCC(CH₃)3)]Cu[P(C₆H₄CH₃)3]⁽¹⁺⁾*PF₆^(1-)=[((CO)3(((C₆H₅)2PCH₂)2)Mn(C₆H₉))Cu(PC₂₁H₂₁)]PF₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

thallium(I) hexafluorophosphate (60969-19-9) + [(CO)3((C6H5)2PCH2CH2P(C6H5)2)Mn(CCC(CH3)3)]CuCl (105560-21-2) + tris-(o-tolyl)phosphine (6163-58-2) → [(CO)3(((C6H5)2PCH2)2)Mn(CCC(CH3)3)]Cu[P(C6H4CH3)3](1+)*PF6(1-)=[((CO)3(((C6H5)2PCH2)2)Mn(C6H9))Cu(PC21H21)]PF6 (105560-20-1)

Guidance literature:

In dichloromethane; react. of Cu-Mn complex with P(C6H4Me-2)3 and TlPF6 in CH2Cl2;

DOI:10.1016/0022-328X(86)84019-0

Reference yield:

thallium(I) hexafluorophosphate (60969-19-9) + [MnCuCl(C2C(CH3)3)(CO)3((CH2P(C6H5)2)2)] (105560-21-2) + tris-(o-tolyl)phosphine (6163-58-2) → [MnCu(C2C(CH3)3)(CO)3((CH2P(C6H5)2)2)(P(C6H4CH3)3)](1+)*PF6(1-)=[MnCu(C2C(CH3)3)(CO)3((CH2P(C6H5)2)2)(P(C6H4CH3)3)]PF6 (105560-20-1)

Guidance literature:

In dichloromethane; byproducts: (Cu(P(C6H4Me-2)3)(x))PF6; under Ar, to soln. of MnCuCl(t-BuCC)(CO)3(dppe) and P(C6H4Me-2)3 (1:1.6mole ratio) in CH2Cl2 solid TlPF6 is added, stirred for 5 h; filtered, concd., product pptd. by addn. of Et2O; elem. anal.;

upstream raw materials:

thallium(I) hexafluorophosphate

[MnCuCl(C₂C(CH₃)3)(CO)3((CH₂P(C₆H₅)2)2)]

tris-(o-tolyl)phosphine

[(CO)3((C₆H₅)2PCH₂CH₂P(C₆H₅)2)Mn(CCC(CH₃)3)]CuCl