(C₆H₅)4Sb⁽¹⁺⁾*BCl₄^(1-)=(C₆H₅)4SbBCl₄

Base Information

• Chemical Name: (C₆H₅)4Sb⁽¹⁺⁾*BCl₄^(1-)=(C₆H₅)4SbBCl₄
• CAS No.: 84239-06-5
• Molecular Formula: BCl₄*C₂₄H₂₀Sb
• Molecular Weight: 582.796
• Mol file: 84239-06-5.mol

Synonyms:

Chemical Property of (C₆H₅)4Sb⁽¹⁺⁾*BCl₄^(1-)=(C₆H₅)4SbBCl₄

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

Useful:

Technology Process of (C₆H₅)4Sb⁽¹⁺⁾*BCl₄^(1-)=(C₆H₅)4SbBCl₄

There total 1 articles about (C₆H₅)4Sb⁽¹⁺⁾*BCl₄^(1-)=(C₆H₅)4SbBCl₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

tetraphenylantimony(V) chloride (19638-17-6,16894-68-1) + boron trichloride (10294-34-5) → (C6H5)4Sb(1+)*BCl4(1-)=(C6H5)4SbBCl4 (84239-06-5)

Guidance literature:

In benzene; to dry benzene (or alcoholic) soln. of BCl3 was added slowly benzene (or alcoholic) soln. of Ph4SbCl at 0°C under dry N2 atm., with vigorous shaking, N2 gas was passed through for 6-10 h, molar ratio=1:1; flask stoppered and kept aside for a day or two, supernatant was decanted off, solid product was washed successively with dry benzene and dry n-hexane, dried in vac. at room temp., elem. anal.;

upstream raw materials:

tetraphenylantimony(V) chloride

boron trichloride