2,3,4,9-Tetrahydro-8-methyl-1H-carbazole

Base Information

Chemical Name:2,3,4,9-Tetrahydro-8-methyl-1H-carbazole
CAS No.:19283-51-3
Molecular Formula:C13H15 N
Molecular Weight:185.269
Hs Code.:2933990090
European Community (EC) Number:242-935-9
UNII:LWK8Z87M8H
DSSTox Substance ID:DTXSID30172880
Nikkaji Number:J242.758C
Wikidata:Q83042954
Mol file:19283-51-3.mol

Synonyms:2,3,4,9-Tetrahydro-8-methyl-1H-carbazole;19283-51-3;8-methyl-2,3,4,9-tetrahydro-1H-carbazole;EINECS 242-935-9;1,2,3,4-Tetrahydro-8-methylcarbazole;LWK8Z87M8H;DTXSID30172880;YSOBXTJUYFKXDF-UHFFFAOYSA-N;STK945061;AKOS000275070;8-methyl-1,2,3,4-tetrahydrocarbazole;Carbazole, 1,2,3,4-tetrahydro-8-methyl-;1-Methyl-5,6,7,8-tetrahydro-9H-carbazole;1H-Carbazole, 2,3,4,9-tetrahydro-8-methyl-

Suppliers and Price of 2,3,4,9-Tetrahydro-8-methyl-1H-carbazole

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 5 raw suppliers

Chemical Property of 2,3,4,9-Tetrahydro-8-methyl-1H-carbazole

Chemical Property:

Vapor Pressure:0.000242mmHg at 25°C
Boiling Point:334.8°C at 760 mmHg
Flash Point:145.2°C
PSA：15.79000
Density:1.122g/cm³
LogP:3.35510
XLogP3:3.6
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:0
Rotatable Bond Count:0
Exact Mass:185.120449483
Heavy Atom Count:14
Complexity:213

Purity/Quality:: 98%Min ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=C2C(=CC=C1)C3=C(N2)CCCC3

Technology Process of 2,3,4,9-Tetrahydro-8-methyl-1H-carbazole

There total 22 articles about 2,3,4,9-Tetrahydro-8-methyl-1H-carbazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 108-94-1,11119-77-0,9003-41-2,9075-99-4
cyclohexanone

: 529-27-1
2-methylphenylhydrazine

: 19283-51-3
8-Methyl-1,2,3,4-tetrahydro-carbazol

Guidance literature:: With liquid 1-butyl-3-methylimidazolium hydrosulfate; at 70 ℃; for 0.5h;
DOI:10.1002/ejoc.200600886

Reference yield: 85.0%

: 635-26-7
o-tolylhydrazine hydrochloride

: 108-94-1,11119-77-0,9003-41-2,9075-99-4
cyclohexanone

: 19283-51-3
8-Methyl-1,2,3,4-tetrahydro-carbazol

Guidance literature:: With ammonium cerium (IV) nitrate; In methanol; for 1h; Reflux;
DOI:10.1080/00397910802370719

Reference yield: 83.0%

: 286-20-4
cyclohexane-1,2-epoxide

: 95-53-4
o-toluidine

: 19283-51-3
8-Methyl-1,2,3,4-tetrahydro-carbazol

Guidance literature:: With 1,1'-bis-(diphenylphosphino)ferrocene; dodecacarbonyl-triangulo-triruthenium; toluene-4-sulfonic acid; In 1,4-dioxane; at 150 ℃; for 22h; Inert atmosphere;
DOI:10.1002/chem.201304432