8-methyl-2,3,4,9-tetrahydro-1H-carbazol-1-one

Base Information

Chemical Name:8-methyl-2,3,4,9-tetrahydro-1H-carbazol-1-one
CAS No.:3449-50-1
Molecular Formula:C13H13NO
Molecular Weight:199.252
Hs Code.:2933990090
DSSTox Substance ID:DTXSID401254509
Nikkaji Number:J3.314.402D
Mol file:3449-50-1.mol

Synonyms:8-methyl-2,3,4,9-tetrahydro-1H-carbazol-1-one;3449-50-1;8-methyl-2,3,4,9-tetrahydrocarbazol-1-one;DTXSID401254509;MFCD16090101;AKOS005659163;AS-65177;CS-0061212;A12439;EN300-186556;2,3,4,9-Tetrahydro-8-methyl-1H-carbazol-1-one;Z1201628557

Suppliers and Price of 8-methyl-2,3,4,9-tetrahydro-1H-carbazol-1-one

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

TRC
8-methyl-2,3,4,9-tetrahydro-1H-carbazol-1-one
250mg
$ 285.00

TRC
8-methyl-2,3,4,9-tetrahydro-1H-carbazol-1-one
50mg
$ 65.00

AK Scientific
8-methyl-2,3,4,9-tetrahydrocarbazol-1-one
1g
$ 388.40

AK Scientific
8-methyl-2,3,4,9-tetrahydrocarbazol-1-one
50mg
$ 131.60

Total 11 raw suppliers

Chemical Property of 8-methyl-2,3,4,9-tetrahydro-1H-carbazol-1-one

Chemical Property:

PSA：32.86000
LogP:2.99530
XLogP3:2.8
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:0
Exact Mass:199.099714038
Heavy Atom Count:15
Complexity:276

Purity/Quality:

97% ^*data from raw suppliers

8-methyl-2,3,4,9-tetrahydro-1H-carbazol-1-one ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=C2C(=CC=C1)C3=C(N2)C(=O)CCC3

Technology Process of 8-methyl-2,3,4,9-tetrahydro-1H-carbazol-1-one

There total 1 articles about 8-methyl-2,3,4,9-tetrahydro-1H-carbazol-1-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 635-26-7
o-tolylhydrazine hydrochloride

: 6946-05-0
2-aminocyclohexanone hydrochloride

: 3449-50-1
8-methyl-2,3,4,9-tetrahydro-carbazol-1-one

Guidance literature:: o-tolylhydrazine hydrochloride; 2-aminocyclohexanone hydrochloride; With sodium hydroxide; water; at 20 ℃; for 0.25h;

With water; acetic acid; for 5h; Reflux;
DOI:10.1080/00397910802499567

Reference yield: 90.0%

: 3449-50-1
8-methyl-2,3,4,9-tetrahydro-carbazol-1-one

: 104-87-0
4-methyl-benzaldehyde

: 109-77-3
malononitrile

: 2-amino-10-methyl-4-(4'-methylphenyl)-4,5,6-trihydro-11H-pyrano[2,3-a]carbazole-3-carbonitrile

Guidance literature:: With piperidine; In N,N-dimethyl-formamide; at 120 ℃; for 3h;
DOI:10.1080/00397911.2014.956368

Reference yield: 89.0%

: 3449-50-1
8-methyl-2,3,4,9-tetrahydro-carbazol-1-one

: 2029-94-9
3,4-diethoxybenzaldehyde

: 2-(3',4'-diethoxybenzylidene)-8-methyl-2,3,4,9-tetrahydrocarbazol-1-one

Guidance literature:: With potassium hydroxide; In neat (no solvent); at 20 ℃; for 0.166667h; Milling; Green chemistry;
DOI:10.1016/j.bioorg.2014.03.003