4-Chlorobenzoic acid phenacyl ester

Base Information

Chemical Name:4-Chlorobenzoic acid phenacyl ester
CAS No.:54797-45-4
Molecular Formula:C15H11 Cl O3
Molecular Weight:274.704
Hs Code.:
Mol file:54797-45-4.mol

Synonyms:Benzoylmethyl4-chlorobenzoate; NSC 79399; Phenacyl p-chlorobenzoate

Suppliers and Price of 4-Chlorobenzoic acid phenacyl ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 5 raw suppliers

Chemical Property of 4-Chlorobenzoic acid phenacyl ester

Chemical Property:

Vapor Pressure:1.02E-07mmHg at 25°C
Melting Point:128-129 °C
Boiling Point:433.5°C at 760 mmHg
Flash Point:178.9°C
PSA：43.37000
Density:1.276g/cm³
LogP:3.37970

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 4-Chlorobenzoic acid phenacyl ester

There total 7 articles about 4-Chlorobenzoic acid phenacyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.1%

: 70-11-1
α-bromoacetophenone

: 74-11-3
para-chlorobenzoic acid

: 54797-45-4
2-oxo-2-phenylethyl-4-chlorobenzoate

Guidance literature:: With sodium carbonate; In ethanol; water; for 1.5h; Heating;
DOI:10.1016/0040-4020(96)00552-2

Reference yield: 76.0%

: 100-42-5,25038-60-2,25247-68-1,28213-80-1,28325-75-9,79637-11-9,9003-53-6
styrene

: 74-11-3
para-chlorobenzoic acid

: 54797-45-4
2-oxo-2-phenylethyl-4-chlorobenzoate

Guidance literature:: With tert.-butylhydroperoxide; iodine; triethylamine; In decane; dimethyl sulfoxide; at 25 ℃; for 12h; regioselective reaction; Inert atmosphere;
DOI:10.1021/ol5027393

Reference yield: 75.0%

: 100-42-5,25038-60-2,25247-68-1,28213-80-1,28325-75-9,79637-11-9,9003-53-6
styrene

: 104-88-1
4-chlorobenzaldehyde

: 54797-45-4
2-oxo-2-phenylethyl-4-chlorobenzoate

Guidance literature:: With N-Bromosuccinimide; oxygen; 3-benzyl-5-(2-hydroxyethyl)-4-methyl-1,3-thiazol-3-ium chloride; triethylamine; In dimethyl sulfoxide; at 25 ℃; for 24h; under 760.051 Torr; regioselective reaction;
DOI:10.1039/c3ob41551a