4-(2-Morpholinoethoxy)naphthalen-1-aMine dihydrochloride

Base Information

• Chemical Name: 4-(2-Morpholinoethoxy)naphthalen-1-aMine dihydrochloride
• CAS No.: 285984-50-1
• Molecular Formula: C16H20N2O2.2ClH
• Molecular Weight: 345.26400
• Hs Code.: 2934999090
• Mol file: 285984-50-1.mol

Synonyms:4-(2-Morpholinoethoxy)naphthalen-1-amine dihydrochloride;

Chemical Property of 4-(2-Morpholinoethoxy)naphthalen-1-aMine dihydrochloride

Chemical Property:

• PSA: 47.72000
• LogP: 4.25610
• Storage Temp.: Sealed in dry,Room Temperature

Purity/Quality:

≥99% ^*data from raw suppliers

4-(2-Morpholinoethoxy)naphthalen-1-amine dihydrochloride 95+% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 4-(2-Morpholinoethoxy)naphthalen-1-aMine dihydrochloride

There total 2 articles about 4-(2-Morpholinoethoxy)naphthalen-1-aMine dihydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

[4-(2-morpholin-4-yl-ethoxy)naphthalen-1-yl]carbamic acid tert-butyl ester (285984-35-2) → 1-amino-4-(2-morpholin-4-yl-ethoxy)naphthalene dihydrochloride (285984-50-1)

Guidance literature:

With hydrogenchloride; In 1,4-dioxane; at 20 ℃; for 20h;

Reference yield:

4-(2-([1]-naphthyloxy-[4]-acetamido)ethyl)morpholine (501083-98-3) → 1-amino-4-(2-morpholin-4-yl-ethoxy)naphthalene dihydrochloride (285984-50-1)

Guidance literature:

With hydrogenchloride; In ethanol; water; isopropyl alcohol;

Reference yield: 91.0%

C16H17Cl3N4O4 (1012883-12-3) + C16H20N2O2*ClH (317806-89-6,285984-50-1) → 1-[2-(3-nitrophenyl)-5-tert-butyl-2H-pyrazol-3-yl]-3-[4-(2-morpholin-4-yl-ethoxy)naphthalen-1-yl]-urea (611168-85-5)

Guidance literature:

C₁₆H₂₀N₂O₂*ClH; With N-ethyl-N,N-diisopropylamine; In dimethyl sulfoxide; at 20 ℃; for 0.166667h;

C₁₆H₁₇Cl₃N₄O₄; In dimethyl sulfoxide; at 60 ℃; for 9h;

DOI:10.1021/jm500167q

upstream raw materials:

[4-(2-morpholin-4-yl-ethoxy)naphthalen-1-yl]carbamic acid tert-butyl ester

4-(2-([1]-naphthyloxy-[4]-acetamido)ethyl)morpholine

Downstream raw materials:

1-(4-chloro-3-(trifluoromethyl)phenyl)-3-(4-(2-morpholinoethoxy)-naphthalen-1-yl)urea

1-(1-(3-aminophenyl)-3-(tert-butyl)-1H-pyrazol-5-yl)-3-(4-(2-morpholinoethoxy)naphthalen-1-yl)urea

1-(3-(tert-butyl)-1-(3-((2-ethoxyethyl)amino)phenyl)-1H-pyrazol-5-yl)-3-(4-(2-morpholinoethoxy)naphthalen-1-yl)urea

N-(3-(3-(tert-butyl)-5-(3-(4-(2-morpholinoethoxy)naphthalen-1-yl)ureido)-1H-pyrazol-1-yl)phenyl)propionamide

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